C₂₂H₂₈O₂Si

Base Information

Chemical Name:C₂₂H₂₈O₂Si
CAS No.:1354913-35-1
Molecular Formula:C₂₂H₂₈O₂Si
Molecular Weight:352.549
Hs Code.:

C<sub>22</sub>H<sub>28</sub>O<sub>2</sub>Si

Synonyms:C₂₂H₂₈O₂Si

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Chemical Property of C₂₂H₂₈O₂Si

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Technology Process of C₂₂H₂₈O₂Si

There total 5 articles about C₂₂H₂₈O₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 858132-44-2
(2E,4R)-4-([tert-butyl(diphenyl)silyl]oxy)-2-methylpent-2-en-1-ol

: 1354913-35-1
C₂₂H₂₈O₂Si

Guidance literature:: (2E,4R)-4-([tert-butyl(diphenyl)silyl]oxy)-2-methylpent-2-en-1-ol; With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutyl-ammonium chloride; sodium hydrogencarbonate; potassium carbonate; In dichloromethane; water; at 20 ℃; for 0.166667h;

With N-chloro-succinimide; In dichloromethane; water; at 20 ℃; for 5h;
DOI:10.1039/c1ob06559a

Reference yield:

: 561038-05-9
(R)-2-(tert-butyldiphenylsilanyloxy)propionic acid methyl ester

: 1354913-35-1
C₂₂H₂₈O₂Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: diisobutylaluminium hydride / dichloromethane; toluene / 1 h / -78 °C

2.1: dichloromethane / 18 h / 20 °C

3.1: diisobutylaluminium hydride / dichloromethane; toluene / 1 h / -78 °C

4.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutyl-ammonium chloride; sodium hydrogencarbonate; potassium carbonate / dichloromethane; water / 0.17 h / 20 °C

4.2: 5 h / 20 °C

With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutyl-ammonium chloride; diisobutylaluminium hydride; sodium hydrogencarbonate; potassium carbonate; In dichloromethane; water; toluene; 2.1: Wittig olefination;
DOI:10.1039/c1ob06559a

Reference yield:

: 858132-43-1
ethyl (2E,4R)-4-([tert-butyl(diphenyl)silyl]oxy)-2-methylpent-2-enoate

: 1354913-35-1
C₂₂H₂₈O₂Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: diisobutylaluminium hydride / dichloromethane; toluene / 1 h / -78 °C

2.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutyl-ammonium chloride; sodium hydrogencarbonate; potassium carbonate / dichloromethane; water / 0.17 h / 20 °C

2.2: 5 h / 20 °C

With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutyl-ammonium chloride; diisobutylaluminium hydride; sodium hydrogencarbonate; potassium carbonate; In dichloromethane; water; toluene;
DOI:10.1039/c1ob06559a