C₂₈H₄₂O₆Si

Base Information

• Chemical Name: C₂₈H₄₂O₆Si
• CAS No.: 113706-74-4
• Molecular Formula: C₂₈H₄₂O₆Si
• Molecular Weight: 502.723
• Mol file: 113706-74-4.mol

Synonyms:C₂₈H₄₂O₆Si

Chemical Property of C₂₈H₄₂O₆Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₈H₄₂O₆Si

There total 4 articles about C₂₈H₄₂O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

benzyl bromide (100-39-0) + C21H36O6Si (113706-67-5) → C28H42O6Si (113706-74-4)

Guidance literature:

With sodium hydride; In tetrahydrofuran; for 1h; Heating;

DOI:10.1016/S0040-4039(00)96173-2

Reference yield:

C30H48O9Si (113725-82-9) → C28H42O6Si (113706-74-4)

Guidance literature:

Multi-step reaction with 2 steps

1: NaOMe / methanol / Ambient temperature

2: 86 percent / NaH / tetrahydrofuran / 1 h / Heating

With sodium methylate; sodium hydride; In tetrahydrofuran; methanol;

DOI:10.1016/S0040-4039(00)96173-2

Reference yield:

T-2 toxin (21259-20-1) → C28H42O6Si (113706-74-4)

Guidance literature:

Multi-step reaction with 3 steps

1: 95 percent / imidazole / dimethylformamide

2: NaOMe / methanol / Ambient temperature

3: 86 percent / NaH / tetrahydrofuran / 1 h / Heating

With 1H-imidazole; sodium methylate; sodium hydride; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;

DOI:10.1016/S0040-4039(00)96173-2

upstream raw materials:

benzyl bromide

C₂₁H₃₆O₆Si

C₃₀H₄₈O₉Si

T-2 toxin

Downstream raw materials:

C₃₆H₅₆O₉Si

C₃₂H₄₆O₁₀

C₃₀H₄₂O₉

C₃₈H₆₀O₁₀Si

Refernces