Technology Process of C17H24O7
There total 1 articles about C17H24O7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydride;
In
N,N-dimethyl-formamide;
at 0 - 20 ℃;
DOI:10.1021/ol990281j
- Guidance literature:
-
With
lithium aluminium tetrahydride; aluminium trichloride;
In
tetrahydrofuran;
for 8h;
Heating;
DOI:10.1021/ol990281j
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 62 percent / lithium aluminum hydride; aluminum chloride / tetrahydrofuran / 8 h / Heating
2.1: dimethyl sulfoxide; oxalyl chloride; ethyldiisopropylamine / CH2Cl2 / -78 - 20 °C
3.1: lithium diisopropylamide / tetrahydrofuran / 0.25 h / 0 °C
3.2: 17 mg / tetrahydrofuran / 16 h / 20 °C
With
lithium aluminium tetrahydride; aluminium trichloride; oxalyl dichloride; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; lithium diisopropyl amide;
In
tetrahydrofuran; dichloromethane;
2.1: Swern oxidation / 3.2: Horner-Wadsworth-Emmons reaction;
DOI:10.1021/ol990281j