O-(4-BROMOBENZYL)HYDROXYLAMINE HYDROCHLORIDE

Base Information

• Chemical Name: O-(4-BROMOBENZYL)HYDROXYLAMINE HYDROCHLORIDE
• CAS No.: 40780-59-4
• Molecular Formula: C7H8 Br N O . Cl H
• Molecular Weight: 238.512
• Hs Code.: 2922199090
• Mol file: 40780-59-4.mol

Synonyms:Benzyloxyamine,p-bromo-, hydrochloride (6CI); Hydroxylamine, O-[(4-bromophenyl)methyl]-, hydrochloride(9CI)

Chemical Property of O-(4-BROMOBENZYL)HYDROXYLAMINE HYDROCHLORIDE

Chemical Property:

• PSA: 35.25000
• LogP: 3.34170

Purity/Quality:

99% ^*data from raw suppliers

O-(4-Bromobenzyl)hydroxylaminehydrochloride 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of O-(4-BROMOBENZYL)HYDROXYLAMINE HYDROCHLORIDE

There total 8 articles about O-(4-BROMOBENZYL)HYDROXYLAMINE HYDROCHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.85%

O-(p-bromobenzyl)acetoxime → O-(4-Bromobenzyl)hydroxylamine hydrochloride (40780-59-4)

Guidance literature:

With hydrogenchloride; In methanol; water; at 38 ℃; for 3.5h;

Reference yield: 85.0%

1-(4-bromobenzyloxy)-3,4-diphenyl-1H-pyrrole-2,5-dione → 2,3-diphenylmaleic anhydride (4808-48-4) + O-(4-Bromobenzyl)hydroxylamine hydrochloride (40780-59-4)

Guidance literature:

1-(4-bromobenzyloxy)-3,4-diphenyl-1H-pyrrole-2,5-dione; With potassium hydroxide; In ethanol; water; at 102 ℃; for 0.0833333h; Microwave irradiation; Green chemistry;

With hydrogenchloride; In ethanol; water; pH=4; Temperature; Green chemistry;

DOI:10.1039/c6gc01318j

Reference yield: 67.0%

2-((4-bromobenzyl)oxy)isoindoline-1,3-dione (55418-33-2) → O-(4-Bromobenzyl)hydroxylamine hydrochloride (40780-59-4)

Guidance literature:

2-((4-bromobenzyl)oxy)isoindoline-1,3-dione; With hydrazine hydrate; In dichloromethane; at 0 - 20 ℃; for 2h;

With hydrogenchloride; In 1,4-dioxane; at 0 ℃;

upstream raw materials:

2-((4-bromobenzyl)oxy)isoindoline-1,3-dione

1-bromomethyl-4-bromobenzene

O-(4-bromobenzyl)hydroxylamine

p-bromobenzyl chloride