(E)-1-(4-{1-[3,5-dimethyl-4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-1-ethylpropyl}-2-methyl-phenyl)-3-ethyl-1-penten-3-ol

Base Information

Chemical Name:(E)-1-(4-{1-[3,5-dimethyl-4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-1-ethylpropyl}-2-methyl-phenyl)-3-ethyl-1-penten-3-ol
CAS No.:917023-02-0
Molecular Formula:C₃₃H₄₉BO₃
Molecular Weight:504.561
Hs Code.:

Synonyms:(E)-1-(4-{1-[3,5-dimethyl-4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-1-ethylpropyl}-2-methyl-phenyl)-3-ethyl-1-penten-3-ol

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Chemical Property of (E)-1-(4-{1-[3,5-dimethyl-4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-1-ethylpropyl}-2-methyl-phenyl)-3-ethyl-1-penten-3-ol

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Technology Process of (E)-1-(4-{1-[3,5-dimethyl-4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-1-ethylpropyl}-2-methyl-phenyl)-3-ethyl-1-penten-3-ol

There total 6 articles about (E)-1-(4-{1-[3,5-dimethyl-4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-1-ethylpropyl}-2-methyl-phenyl)-3-ethyl-1-penten-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 917024-96-5
trifluoromethanesulfonic acid 4-{1-ethyl-1-[(E)-4-(3-ethyl-3-hydroxy-1-pentenyl)-3-methyl-phenyl]-propyl}-2,6-dimethyl-phenyl ester

: 73183-34-3
bis(pinacol)diborane

: 917023-02-0
(E)-1-(4-{1-[3,5-dimethyl-4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-1-ethylpropyl}-2-methyl-phenyl)-3-ethyl-1-penten-3-ol

Guidance literature:: With potassium acetate; 1,1'-bis-(diphenylphosphino)ferrocene; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In 1,4-dioxane; at 90 ℃;

Reference yield:

: 854502-97-9
3-(4-bromo-3-methyl-phenyl)-pentan-3-ol

: 917023-02-0
(E)-1-(4-{1-[3,5-dimethyl-4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-1-ethylpropyl}-2-methyl-phenyl)-3-ethyl-1-penten-3-ol

Guidance literature:: Multi-step reaction with 5 steps

1: trifluoroacetic acid / 2 h / 20 °C

2: triethylamine / bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / 0.05 h / 160 °C / Irradiation

3: sodium bis(2-methoxyethoxy)aluminium dihydride / tetrahydrofuran; toluene / 2 h / 0 °C

4: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.17 h / -40 °C

5: potassium acetate / 1,1'-bis-(diphenylphosphino)ferrocene; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 90 °C

With potassium acetate; triethylamine; N-ethyl-N,N-diisopropylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; trifluoroacetic acid; bis-triphenylphosphine-palladium(II) chloride; 1,1'-bis-(diphenylphosphino)ferrocene; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) iodide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; toluene;

Reference yield:

: 865239-54-9
4-{1-ethyl-1-[(E)-4-(3-ethyl-3-hydroxy-1-pentenyl)-3-methyl-phenyl]-propyl}-2,6-dimethyl-phenol

: 917023-02-0
(E)-1-(4-{1-[3,5-dimethyl-4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-1-ethylpropyl}-2-methyl-phenyl)-3-ethyl-1-penten-3-ol

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.17 h / -40 °C

2: potassium acetate / 1,1'-bis-(diphenylphosphino)ferrocene; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 90 °C

With potassium acetate; N-ethyl-N,N-diisopropylamine; 1,1'-bis-(diphenylphosphino)ferrocene; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In 1,4-dioxane; dichloromethane;