diethyl cyclohexylethynylphosphonate

Base Information

Chemical Name:diethyl cyclohexylethynylphosphonate
CAS No.:30238-20-1
Molecular Formula:C₁₂H₂₁O₃P
Molecular Weight:244.271
Hs Code.:

Synonyms:diethyl cyclohexylethynylphosphonate

Suppliers and Price of diethyl cyclohexylethynylphosphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl cyclohexylethynylphosphonate

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Technology Process of diethyl cyclohexylethynylphosphonate

There total 3 articles about diethyl cyclohexylethynylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: (2-cyclohexyl-ethynesulfonyl)-benzene

: 122-52-1
triethyl phosphite

: 599-70-2
ethyl phenyl sulfone

: 30238-20-1
diethyl cyclohexylethynylphosphonate

Guidance literature:: In tetrahydrofuran; at 60 ℃; for 3h;
DOI:10.1016/j.tetlet.2008.02.013

Reference yield: 48.0%

: 931-48-6
2-cyclohexylacetylene

: 814-49-3
diethyl chlorophosphate

: 30238-20-1
diethyl cyclohexylethynylphosphonate

Guidance literature:: 2-cyclohexylacetylene; With diisopropylamine; lithium diisopropyl amide; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 2h; Inert atmosphere;

diethyl chlorophosphate; In tetrahydrofuran; hexane; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1021/jo9010206