(E)-diethyl cyclohex-2-enylidenemethylphosphonate

Base Information

Chemical Name:(E)-diethyl cyclohex-2-enylidenemethylphosphonate
CAS No.:78463-01-1
Molecular Formula:C₁₂H₂₁O₃P
Molecular Weight:244.271
Hs Code.:

Synonyms:(E)-diethyl cyclohex-2-enylidenemethylphosphonate

Suppliers and Price of (E)-diethyl cyclohex-2-enylidenemethylphosphonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (E)-diethyl cyclohex-2-enylidenemethylphosphonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (E)-diethyl cyclohex-2-enylidenemethylphosphonate

There total 5 articles about (E)-diethyl cyclohex-2-enylidenemethylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 21983-08-4
diethyl (2-cyclohex-1-en-1-yl)ethynylphosphonate

: ((Z)-2-Cyclohex-1-enyl-vinyl)-phosphonic acid diethyl ester

: 78463-01-1
(E)-diethyl cyclohex-2-enylidenemethylphosphonate

Guidance literature:: With sodium tetrahydroborate; indium(III) chloride; In acetonitrile; at -15 - 20 ℃; for 15h;
DOI:10.1016/j.jorganchem.2005.01.024

Reference yield: 82.0%

: 1660-94-2
Tetraethyl methylenediphosphonate

: 1192-88-7
1-cyclohexene-1-carboxaldehyde

: 78463-01-1
(E)-diethyl cyclohex-2-enylidenemethylphosphonate

Guidance literature:: Tetraethyl methylenediphosphonate; With sodium hydride; In toluene; at 20 ℃; for 0.25h; Inert atmosphere;

1-cyclohexene-1-carboxaldehyde; In toluene; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.tet.2012.11.059

Reference yield: 45.0%

: 30238-20-1
diethyl cyclohexylethynylphosphonate

: 78463-01-1
(E)-diethyl cyclohex-2-enylidenemethylphosphonate

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; at 100 - 135 ℃; for 5h; Inert atmosphere;
DOI:10.3987/COM-10-S(E)12