1,3-dimethyl 2-(but-3-enyl)-2-(3-(4-methoxyphenyl)prop-2-yn-1-yl)malonate

Base Information

Chemical Name:1,3-dimethyl 2-(but-3-enyl)-2-(3-(4-methoxyphenyl)prop-2-yn-1-yl)malonate
CAS No.:1392011-66-3
Molecular Formula:C₁₉H₂₂O₅
Molecular Weight:330.381
Hs Code.:

Synonyms:1,3-dimethyl 2-(but-3-enyl)-2-(3-(4-methoxyphenyl)prop-2-yn-1-yl)malonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3-dimethyl 2-(but-3-enyl)-2-(3-(4-methoxyphenyl)prop-2-yn-1-yl)malonate

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Technology Process of 1,3-dimethyl 2-(but-3-enyl)-2-(3-(4-methoxyphenyl)prop-2-yn-1-yl)malonate

There total 1 articles about 1,3-dimethyl 2-(but-3-enyl)-2-(3-(4-methoxyphenyl)prop-2-yn-1-yl)malonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 5162-44-7
1-bromo-4-butene

: 1092400-70-8
2-(3-(p-methoxyphenyl)prop-2-ynyl)malonic acid dimethyl ester

: 1392011-66-3
1,3-dimethyl 2-(but-3-enyl)-2-(3-(4-methoxyphenyl)prop-2-yn-1-yl)malonate

Guidance literature:: 2-(3-(p-methoxyphenyl)prop-2-ynyl)malonic acid dimethyl ester; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 - 23 ℃; for 0.5h; Inert atmosphere;

1-bromo-4-butene; In N,N-dimethyl-formamide; mineral oil; Inert atmosphere;
DOI:10.1039/c2ob25419k

Reference yield: 80.0%

: 1392011-66-3
1,3-dimethyl 2-(but-3-enyl)-2-(3-(4-methoxyphenyl)prop-2-yn-1-yl)malonate

: 1392011-67-4
3,3-dimethyl 8-(4-methoxyphenyl)bicyclo[4.2.0]oct-1⁽⁸⁾-ene-3,3-dicarboxylate

Guidance literature:: With JohnPhosAu(MeCN)SbF₆; In dichloromethane; at 80 ℃; for 15h; Inert atmosphere; Microwave irradiation;
DOI:10.1039/c2ob25419k