3-(3-methoxy-4-hydroxyphenyl)propyl 2-acetamido-2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:3-(3-methoxy-4-hydroxyphenyl)propyl 2-acetamido-2-deoxy-β-D-glucopyranoside
CAS No.:1338496-36-8
Molecular Formula:C₁₈H₂₇NO₈
Molecular Weight:385.414
Hs Code.:

Synonyms:3-(3-methoxy-4-hydroxyphenyl)propyl 2-acetamido-2-deoxy-β-D-glucopyranoside

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Chemical Property of 3-(3-methoxy-4-hydroxyphenyl)propyl 2-acetamido-2-deoxy-β-D-glucopyranoside

Chemical Property:

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Technology Process of 3-(3-methoxy-4-hydroxyphenyl)propyl 2-acetamido-2-deoxy-β-D-glucopyranoside

There total 4 articles about 3-(3-methoxy-4-hydroxyphenyl)propyl 2-acetamido-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1338496-33-5
3-(3-methoxy-4-benzyloxyphenyl)propyl 2-acetamido-2-deoxy-β-D-glucopyranoside

: 1338496-36-8
3-(3-methoxy-4-hydroxyphenyl)propyl 2-acetamido-2-deoxy-β-D-glucopyranoside

Guidance literature:: With 5%-palladium/activated carbon; ammonium formate; In methanol; for 6h; Reflux;
DOI:10.1016/j.bmc.2011.07.031

Reference yield:

: 1338496-24-4
C₃₁H₃₉NO₁₁

: 1338496-36-8
3-(3-methoxy-4-hydroxyphenyl)propyl 2-acetamido-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium methylate / methanol / 2 h / 20 °C

1.2: Amberlite IRA-120 / 20 °C / pH 7

2.1: 5%-palladium/activated carbon; ammonium formate / methanol / 6 h / Reflux

With 5%-palladium/activated carbon; ammonium formate; sodium methylate; In methanol;
DOI:10.1016/j.bmc.2011.07.031

Reference yield:

: 57371-44-5
3-<4-(benzyloxy)-3-methoxyphenyl>propan-1-ol

: 1338496-36-8
3-(3-methoxy-4-hydroxyphenyl)propyl 2-acetamido-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: 4,4'-dimethoxytrityl chloride; zinc(II) chloride / dichloromethane / 20 °C

2.1: sodium methylate / methanol / 2 h / 20 °C

2.2: Amberlite IRA-120 / 20 °C / pH 7

3.1: 5%-palladium/activated carbon; ammonium formate / methanol / 6 h / Reflux

With 5%-palladium/activated carbon; 4,4'-dimethoxytrityl chloride; ammonium formate; sodium methylate; zinc(II) chloride; In methanol; dichloromethane;
DOI:10.1016/j.bmc.2011.07.031