4-[2-(4-methoxyphenyl)hydrazono]-3-methyl-1-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-1H-pyrazol-5(4H)-one

Base Information

• Chemical Name: 4-[2-(4-methoxyphenyl)hydrazono]-3-methyl-1-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-1H-pyrazol-5(4H)-one
• CAS No.: 1415650-80-4
• Molecular Formula: C₂₅H₃₀N₄O₁₁
• Molecular Weight: 562.533

Synonyms:4-[2-(4-methoxyphenyl)hydrazono]-3-methyl-1-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-1H-pyrazol-5(4H)-one

Chemical Property of 4-[2-(4-methoxyphenyl)hydrazono]-3-methyl-1-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-1H-pyrazol-5(4H)-one

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Technology Process of 4-[2-(4-methoxyphenyl)hydrazono]-3-methyl-1-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-1H-pyrazol-5(4H)-one

There total 1 articles about 4-[2-(4-methoxyphenyl)hydrazono]-3-methyl-1-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-1H-pyrazol-5(4H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

4-[2-(4-methoxyphenyl)hydrazono]-3-methyl-1H-pyrazol-5(4H)-one (65078-63-9) + 2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide (572-09-8) → 4-[2-(4-methoxyphenyl)hydrazono]-3-methyl-1-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-1H-pyrazol-5(4H)-one (1415650-80-4)

Guidance literature:

4-[2-(4-methoxyphenyl)hydrazono]-3-methyl-1H-pyrazol-5(4H)-one; With potassium carbonate; In acetone; at 20 ℃; for 0.5h;

2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide; In acetone; Reflux;

DOI:10.1080/15257770.2012.732250

Reference yield: 83.0%

4-[2-(4-methoxyphenyl)hydrazono]-3-methyl-1-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-1H-pyrazol-5(4H)-one (1415650-80-4) → 1-(β-D-glucopyranosyl)-4-[2-(4-methoxy)phenylhydrazono]-3-methyl-1Hpyrazol-5(4H)-one (1415650-83-7)

Guidance literature:

With triethylamine; In methanol; at 20 ℃;

DOI:10.1080/15257770.2012.732250

upstream raw materials:

4-[2-(4-methoxyphenyl)hydrazono]-3-methyl-1H-pyrazol-5(4H)-one

2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

Downstream raw materials:

1-(β-D-glucopyranosyl)-4-[2-(4-methoxy)phenylhydrazono]-3-methyl-1Hpyrazol-5(4H)-one

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