N₃-benzoyl-2'-O-methoxycarbonylmethyl-1',3'-O-(1,1,3,3-tetraisopropyldisiloxane)uridine

Base Information

• Chemical Name: N₃-benzoyl-2'-O-methoxycarbonylmethyl-1',3'-O-(1,1,3,3-tetraisopropyldisiloxane)uridine
• CAS No.: 1207847-50-4
• Molecular Formula: C₃₁H₄₆N₂O₁₀Si₂
• Molecular Weight: 662.885

Synonyms:N₃-benzoyl-2'-O-methoxycarbonylmethyl-1',3'-O-(1,1,3,3-tetraisopropyldisiloxane)uridine

Chemical Property of N₃-benzoyl-2'-O-methoxycarbonylmethyl-1',3'-O-(1,1,3,3-tetraisopropyldisiloxane)uridine

Chemical Property:

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Technology Process of N₃-benzoyl-2'-O-methoxycarbonylmethyl-1',3'-O-(1,1,3,3-tetraisopropyldisiloxane)uridine

There total 1 articles about N₃-benzoyl-2'-O-methoxycarbonylmethyl-1',3'-O-(1,1,3,3-tetraisopropyldisiloxane)uridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

3-benzoyl-1-[(6aR,8R,9R,9aS)-9-hydroxy-2,2,4,4-tetraisopropyltetrahydro-6H-furo[3,2-f][1,3,5,2,4]trioxadisilocin-8-yl]pyrimidine-2,4(1H,3H)-dione (86988-35-4) + bromoacetic acid methyl ester (96-32-2) → N3-benzoyl-2'-O-methoxycarbonylmethyl-1',3'-O-(1,1,3,3-tetraisopropyldisiloxane)uridine (1207847-50-4)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 6.5h; Inert atmosphere;

DOI:10.1080/15257770903307185

Reference yield: 62.0%

N3-benzoyl-2'-O-methoxycarbonylmethyl-1',3'-O-(1,1,3,3-tetraisopropyldisiloxane)uridine (1207847-50-4) → N3-benzoyl-2'-O-methoxycarbonylmethyluridine (1207847-51-5)

Guidance literature:

With triethylamine tris(hydrogen fluoride); In tetrahydrofuran; at 20 ℃;

DOI:10.1080/15257770903307185

upstream raw materials:

3-benzoyl-1-[(6aR,8R,9R,9aS)-9-hydroxy-2,2,4,4-tetraisopropyltetrahydro-6H-furo[3,2-f][1,3,5,2,4]trioxadisilocin-8-yl]pyrimidine-2,4(1H,3H)-dione

bromoacetic acid methyl ester

Downstream raw materials:

N₃-benzoyl-2'-O-methoxycarbonylmethyluridine

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