tetra-N-benzyl-3',4':5,6-di-O-cyclohexylidene-tetra-N-methoxycarbonylneamine

Base Information

Chemical Name:tetra-N-benzyl-3',4':5,6-di-O-cyclohexylidene-tetra-N-methoxycarbonylneamine
CAS No.:110537-69-4
Molecular Formula:C₆₀H₇₄N₄O₁₄
Molecular Weight:1075.27
Hs Code.:

Synonyms:tetra-N-benzyl-3',4':5,6-di-O-cyclohexylidene-tetra-N-methoxycarbonylneamine

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Chemical Property of tetra-N-benzyl-3',4':5,6-di-O-cyclohexylidene-tetra-N-methoxycarbonylneamine

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Technology Process of tetra-N-benzyl-3',4':5,6-di-O-cyclohexylidene-tetra-N-methoxycarbonylneamine

There total 1 articles about tetra-N-benzyl-3',4':5,6-di-O-cyclohexylidene-tetra-N-methoxycarbonylneamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 100-39-0
benzyl bromide

: 82472-81-9
3',4':5,6-di-O-cyclohexylidene-tetra-N-methoxycarbonylneamine

: 110537-69-4
tetra-N-benzyl-3',4':5,6-di-O-cyclohexylidene-tetra-N-methoxycarbonylneamine

Guidance literature:: With sodium hydride; N,N-dimethyl-formamide; at 25 ℃; for 24h;
DOI:10.1016/S0008-6215(00)90217-9

Reference yield: 81.0%

: 110537-69-4
tetra-N-benzyl-3',4':5,6-di-O-cyclohexylidene-tetra-N-methoxycarbonylneamine

: 110537-70-7
tetra-N-benzyl-5,6-O-cyclohexylidene-tetra-N-methoxycarbonylneamin

Guidance literature:: With acetic acid; at 56 ℃; for 7h;
DOI:10.1016/S0008-6215(00)90217-9

Reference yield:

: 110537-69-4
tetra-N-benzyl-3',4':5,6-di-O-cyclohexylidene-tetra-N-methoxycarbonylneamine

: 110537-77-4
4-O-(6-amino-2,3,6-trideoxy-α-D-erythro-hexopyranosyl)-1,3-di-N-benzyl-5,6-O-cyclohexylidene-2-deoxystreptamine

Guidance literature:: Multi-step reaction with 9 steps

1: 81 percent / 1:1 acetic acid / 7 h / 56 °C

2: periodic acid / tetrahydrofuran / 1 h

3: 0.15 g / triethylamine / methanol / 24 h / 25 °C

4: 81 percent / sodium methoxide / methanol / 2 h / 70 °C

5: 75 percent / boron trifluoride etherate, triethylamine / CHCl₃ / 2 h / -5 °C

6: 92 mg / hydrogen / 10 percent Pd-C / methanol / 3 h / 1520 Torr

7: 35 mg / MeONa / methanol

8: 1) CCl₄, tris(dimethylamino)phosphine 2) sodium azide / 1) N,N-dimethylformamid, -45 deg C, 1.5 h 2) 60 deg C, 48 h

9: 90 percent hydrazine hydrate / 10 percent Pd-C / propan-2-ol / 38 h / Heating

With tetrachloromethane; sodium azide; boron trifluoride diethyl etherate; hydrogen; sodium methylate; hydrazine hydrate; acetic acid; periodic acid; triethylamine; Hexamethylphosphorous triamide; palladium on activated charcoal; In tetrahydrofuran; methanol; chloroform; isopropyl alcohol;
DOI:10.1016/S0008-6215(00)90217-9