N-(2,4-dimethylpenta-1,4-dien-3-yl)-4-methyl-N-(prop-2-ynyl)benzenesulfonamide

Base Information

Chemical Name:N-(2,4-dimethylpenta-1,4-dien-3-yl)-4-methyl-N-(prop-2-ynyl)benzenesulfonamide
CAS No.:1174402-23-3
Molecular Formula:C₁₇H₂₁NO₂S
Molecular Weight:303.425
Hs Code.:

Synonyms:N-(2,4-dimethylpenta-1,4-dien-3-yl)-4-methyl-N-(prop-2-ynyl)benzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2,4-dimethylpenta-1,4-dien-3-yl)-4-methyl-N-(prop-2-ynyl)benzenesulfonamide

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Technology Process of N-(2,4-dimethylpenta-1,4-dien-3-yl)-4-methyl-N-(prop-2-ynyl)benzenesulfonamide

There total 1 articles about N-(2,4-dimethylpenta-1,4-dien-3-yl)-4-methyl-N-(prop-2-ynyl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 131544-26-8
2,4-dimethyl-3-(N-tosylamino)-1,4-pentadiene

: 106-96-7
propargyl bromide

: 1174402-23-3
N-(2,4-dimethylpenta-1,4-dien-3-yl)-4-methyl-N-(prop-2-ynyl)benzenesulfonamide

Guidance literature:: 2,4-dimethyl-3-(N-tosylamino)-1,4-pentadiene; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.0833333h; Inert atmosphere;

propargyl bromide; In N,N-dimethyl-formamide; toluene; at 0 - 22 ℃; Inert atmosphere;
DOI:10.1021/ja904098h

Reference yield: 70.0%

: 74-85-1
ethene

: 1174402-23-3
N-(2,4-dimethylpenta-1,4-dien-3-yl)-4-methyl-N-(prop-2-ynyl)benzenesulfonamide

: 1174402-24-4
N-(2,4-dimethylpenta-1,4-dien-3-yl)-4-methyl-N-(2-methylbut-3-enyl)benzenesulfonamide

Guidance literature:: With Mo(NC₆H₃(iPr)2)(CHCMe₂Ph)(2,5-dimethylpyrrolide)(O(Br)C₁₀H₉C₁₀H₉(Br)(OTBS)); In benzene; at 22 ℃; for 2h;
DOI:10.1021/ja904098h

Reference yield: 66.0%

: 1174402-23-3
N-(2,4-dimethylpenta-1,4-dien-3-yl)-4-methyl-N-(prop-2-ynyl)benzenesulfonamide

: 1174402-25-5
C₁₇H₂₁NO₂S

Guidance literature:: With ethene; Mo(NC₆H₃(CH(CH₃)2)2)(CHC(CH₃)2C₆H₅)(NC₄H₂(CH₃)2)(OC₁₀H₉BrC₁₀H₉BrOSi(CH₃)2C(CH₃)3); In benzene; at 22 ℃; for 12h; Product distribution / selectivity;