2-(methoxymethoxy)-1,3-propanediyl-bis-L-valinate>

Base Information

• Chemical Name: 2-(methoxymethoxy)-1,3-propanediyl-bis-L-valinate>
• CAS No.: 170700-75-1
• Molecular Formula: C₃₁H₄₂N₂O₁₀
• Molecular Weight: 602.682

Synonyms:2-(methoxymethoxy)-1,3-propanediyl-bis-L-valinate>

Chemical Property of 2-(methoxymethoxy)-1,3-propanediyl-bis-L-valinate>

Chemical Property:

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Technology Process of 2-(methoxymethoxy)-1,3-propanediyl-bis-L-valinate>

There total 1 articles about 2-(methoxymethoxy)-1,3-propanediyl-bis-L-valinate> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

2-[(methoxy)methoxy]propane-1,3-diol (170700-79-5) + (S)-N-(benzyloxycarbonyl)valine (1149-26-4) → 2-(methoxymethoxy)-1,3-propanediyl-bis-L-valinate> (170700-75-1)

Guidance literature:

With dmap; dicyclohexyl-carbodiimide; In tetrahydrofuran; at 27 ℃; for 18h;

DOI:10.1080/15257779508009494

Reference yield: 65.0%

Cytosine (71-30-7) + 2-(methoxymethoxy)-1,3-propanediyl-bis-L-valinate> (170700-75-1) → 2-<(4-amino-1,2-dihydro-2-oxo-1-pyrimidinyl)methoxy>-1,3-propanediyl bis-L-valinate (130914-74-8)

Guidance literature:

With benzenesulfonamide; t-butyldimethylsiyl triflate; In acetonitrile; for 18h; Heating;

DOI:10.1080/15257779508009494

Reference yield:

2,4-O,N-bis(trimethylsilyl)cytosine (18037-10-0) + 2-(methoxymethoxy)-1,3-propanediyl-bis-L-valinate> (170700-75-1) → 2-<(4-amino-1,2-dihydro-2-oxo-1-pyrimidinyl)methoxy>-1,3-propanediyl bis-L-valinate (130914-74-8)

Guidance literature:

With t-butyldimethylsiyl triflate;

DOI:10.1080/15257779508009494

upstream raw materials:

2-[(methoxy)methoxy]propane-1,3-diol

(S)-N-(benzyloxycarbonyl)valine

Downstream raw materials:

2-<(4-amino-1,2-dihydro-2-oxo-1-pyrimidinyl)methoxy>-1,3-propanediyl bis-L-valinate

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