endo-7,14-epoxy-7,7a,13a,14-tetrahydro-14-phenyl-8,13-benzoanthracenedione

Base Information

• Chemical Name: endo-7,14-epoxy-7,7a,13a,14-tetrahydro-14-phenyl-8,13-benzo
• Molecular Formula: C₂₈H₁₈O₃
• Molecular Weight: 402.449

Synonyms:endo-7,14-epoxy-7,7a,13a,14-tetrahydro-14-phenyl-8,13-benzoanthracenedione

Chemical Property of endo-7,14-epoxy-7,7a,13a,14-tetrahydro-14-phenyl-8,13-benzo

Chemical Property:

Purity/Quality:

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Useful:

There total 3 articles about endo-7,14-epoxy-7,7a,13a,14-tetrahydro-14-phenyl-8,13-benzoanthracenedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

1-amino-1,3-dihydro-1-phenylnaphto<1,2-c>furan (114468-87-0) + [1,4]naphthoquinone (130-15-4) → endo-7,14-epoxy-7,7a,13a,14-tetrahydro-14-phenyl-8,13-benzoanthracenedione (114468-93-8)

Guidance literature:

With chloroacetic acid; In toluene; for 1h; Heating;

DOI:10.1021/jo00248a009

Reference yield:

(1-bromo-2-naphthyl)methanol (76635-70-6) → endo-7,14-epoxy-7,7a,13a,14-tetrahydro-14-phenyl-8,13-benzoanthracenedione (114468-93-8)

Guidance literature:

Multi-step reaction with 2 steps

2: 91 percent / monochloroacetic acid / toluene / 1 h / Heating

With chloroacetic acid; In toluene;

DOI:10.1021/jo00248a009

Reference yield:

benzonitrile (100-47-0) → endo-7,14-epoxy-7,7a,13a,14-tetrahydro-14-phenyl-8,13-benzoanthracenedione (114468-93-8)

Guidance literature:

Multi-step reaction with 2 steps

2: 91 percent / monochloroacetic acid / toluene / 1 h / Heating

With chloroacetic acid; In toluene;

DOI:10.1021/jo00248a009

upstream raw materials:

1-amino-1,3-dihydro-1-phenylnaphto<1,2-c>furan

[1,4]naphthoquinone

(1-bromo-2-naphthyl)methanol

benzonitrile

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