1,1-Di(2-pyridyl)-1-methoxy-1-<3-<(tert-butyldimethylsilyl)oxy>phenyl>methane

Base Information

Chemical Name:1,1-Di(2-pyridyl)-1-methoxy-1-<3-<(tert-butyldimethylsilyl)oxy>phenyl>methane
CAS No.:155820-15-8
Molecular Formula:C₂₄H₃₀N₂O₂Si
Molecular Weight:406.6
Hs Code.:

Synonyms:1,1-Di(2-pyridyl)-1-methoxy-1-<3-<(tert-butyldimethylsilyl)oxy>phenyl>methane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,1-Di(2-pyridyl)-1-methoxy-1-<3-<(tert-butyldimethylsilyl)oxy>phenyl>methane

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Technology Process of 1,1-Di(2-pyridyl)-1-methoxy-1-<3-<(tert-butyldimethylsilyl)oxy>phenyl>methane

There total 4 articles about 1,1-Di(2-pyridyl)-1-methoxy-1-<3-<(tert-butyldimethylsilyl)oxy>phenyl>methane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 155820-14-7
1,1-Di(2-pyridyl)-1-<3-<(tert-butyldimethylsilyl)oxy>phenyl>methanol

: 74-88-4
methyl iodide

: 155820-15-8
1,1-Di(2-pyridyl)-1-methoxy-1-<3-<(tert-butyldimethylsilyl)oxy>phenyl>methane

Guidance literature:: With sodium hydride; In tetrahydrofuran; 1.) r.t., 1 h, 2.) r.t., 15 h;
DOI:10.1021/jo00087a012

Reference yield:

: 19437-26-4
2,2'-dipyridyl ketone

: 155820-15-8
1,1-Di(2-pyridyl)-1-methoxy-1-<3-<(tert-butyldimethylsilyl)oxy>phenyl>methane

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / tetrahydrofuran

2: NaOH

With sodium hydroxide; In tetrahydrofuran;
DOI:10.1016/S0040-4039(00)73528-3

Reference yield:

: 65423-56-5
1-bromo-3-[(tert-butyldimethylsilyl)oxy]benzene

: 155820-15-8
1,1-Di(2-pyridyl)-1-methoxy-1-<3-<(tert-butyldimethylsilyl)oxy>phenyl>methane

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Mg, BrCH₂CH₂Br / 1.) THF, 2.) THF, r.t., 16 h

2: 71 percent / NaH / tetrahydrofuran / 1.) r.t., 1 h, 2.) r.t., 15 h

With sodium hydride; magnesium; ethylene dibromide; In tetrahydrofuran;
DOI:10.1021/jo00087a012