2-<2,4-Bis(1,1-dimethylpropyl)phenoxy>hexansaeure(2-hydroxy-5-methoxyanilid)

Base Information

• Chemical Name: 2-<2,4-Bis(1,1-dimethylpropyl)phenoxy>hexansaeure(2-hydroxy-5-methoxyanilid)
• CAS No.: 170029-57-9
• Molecular Formula: C₂₉H₄₃NO₄
• Molecular Weight: 469.665

Synonyms:2-<2,4-Bis(1,1-dimethylpropyl)phenoxy>hexansaeure(2-hydroxy-5-methoxyanilid)

Chemical Property of 2-<2,4-Bis(1,1-dimethylpropyl)phenoxy>hexansaeure(2-hydroxy-5-methoxyanilid)

Chemical Property:

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Technology Process of 2-<2,4-Bis(1,1-dimethylpropyl)phenoxy>hexansaeure(2-hydroxy-5-methoxyanilid)

There total 3 articles about 2-<2,4-Bis(1,1-dimethylpropyl)phenoxy>hexansaeure(2-hydroxy-5-methoxyanilid) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-methoxy-2-nitrophenol (1568-70-3) → 2-<2,4-Bis(1,1-dimethylpropyl)phenoxy>hexansaeure(2-hydroxy-5-methoxyanilid) (170029-57-9)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂ / 10percent Pd/C / dioxane

2: dioxane / 0.25 h / Heating

With hydrogen; palladium on activated charcoal; In 1,4-dioxane;

DOI:10.1002/prac.19953370186

Reference yield:

1,4-dimethoxy-2-nitrobenzene (89-39-4) → 2-<2,4-Bis(1,1-dimethylpropyl)phenoxy>hexansaeure(2-hydroxy-5-methoxyanilid) (170029-57-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 88 percent / LiI, quinoline / 0.25 h / 160 - 170 °C

2: H₂ / 10percent Pd/C / dioxane

3: dioxane / 0.25 h / Heating

With quinoline; hydrogen; lithium iodide; palladium on activated charcoal; In 1,4-dioxane;

DOI:10.1002/prac.19953370186

Reference yield:

2-<2,4-Bis(1,1-dimethylpropyl)phenoxy>hexanoylchlorid (63059-55-2) + 2-amino-4-methoxyphenol (20734-76-3) → 2-<2,4-Bis(1,1-dimethylpropyl)phenoxy>hexansaeure(2-hydroxy-5-methoxyanilid) (170029-57-9)

Guidance literature:

In 1,4-dioxane; for 0.25h; Yield given; Heating;

DOI:10.1002/prac.19953370186

upstream raw materials:

2-<2,4-Bis(1,1-dimethylpropyl)phenoxy>hexanoylchlorid

2-amino-4-methoxyphenol

4-methoxy-2-nitrophenol

1,4-dimethoxy-2-nitrobenzene

Downstream raw materials:

2-<2,4-Bis(1,1-dimethylpropyl)phenoxy>hexansaeure(5-methoxy-2-methoxycarbonylmethoxy)-anilid

2-<2,4-Bis(1,1-dimethylpropyl)phenoxy>hexansaeure(5-methoxy-2-methoxycarbonylmethoxy)-4-nitranilid

2-<2,4-Bis(1,1-dimethylpropyl)phenoxy>hexansaeure(5-hydroxy-2-methoxycarbonylmethoxy-4-nitranilid)

(5-Amino-2-{2-[2,4-bis-(1,1-dimethyl-propyl)-phenoxy]-hexanoylamino}-4-hydroxy-phenoxy)-acetic acid methyl ester

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