C₄₅H₆₈O₁₀

Base Information

Chemical Name:C₄₅H₆₈O₁₀
CAS No.:1312441-99-8
Molecular Formula:C₄₅H₆₈O₁₀
Molecular Weight:769.029
Hs Code.:

C<sub>45</sub>H<sub>68</sub>O<sub>10</sub>

Synonyms:C₄₅H₆₈O₁₀

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Chemical Property of C₄₅H₆₈O₁₀

Chemical Property:

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Technology Process of C₄₅H₆₈O₁₀

There total 17 articles about C₄₅H₆₈O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1312441-96-5
C₅₅H₇₄O₁₀S₂

: 1312441-99-8
C₄₅H₆₈O₁₀

Guidance literature:: With hydrogen; In ethanol; at 50 ℃; for 40h;
DOI:10.1021/ol201426c

Reference yield:

: 1312441-87-4
C₁₁H₂₀O₃

: 1312441-99-8
C₄₅H₆₈O₁₀

Guidance literature:: Multi-step reaction with 12 steps

1.1: triethylamine; (-)-diisopinocamphenylborane chloride / diethyl ether / 1 h / 0 °C

1.2: 18 h / -78 - -20 °C

2.1: tetramethylammonium triacetoxyborohydride / acetic acid; acetonitrile / 4 h / -20 - 25 °C

3.1: pyridinium p-toluenesulfonate / dichloromethane / 2 h / 0 - 25 °C

4.1: diisobutylaluminium hydride / toluene / 1 h / -20 °C

5.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 24 h / 25 °C

6.1: pyridinium p-toluenesulfonate / methanol; chloroform / 48 h / 25 °C

7.1: sodium hydride / tetrahydrofuran; mineral oil / 0.33 h / 0 °C

7.2: 6 h / 25 °C

8.1: tert.-butyl lithium / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; pentane / 0.08 h / -78 °C

8.2: 1 h / -78 °C

9.1: manganese(IV) oxide / dichloromethane / 8 h / 25 °C

10.1: 4-toluenesulfonyl azide; potassium carbonate / acetonitrile / 2 h / 25 °C

10.2: 18 h / 25 °C

11.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C

11.2: 0.5 h / -78 - 25 °C

11.3: 3 h / Reflux

12.1: hydrogen / ethanol / 40 h / 50 °C

With manganese(IV) oxide; 4-toluenesulfonyl azide; hydrogen; tert.-butyl lithium; sodium hexamethyldisilazane; pyridinium p-toluenesulfonate; sodium hydride; diisobutylaluminium hydride; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; (-)-diisopinocamphenylborane chloride; tetramethylammonium triacetoxyborohydride; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; ethanol; dichloromethane; chloroform; acetic acid; toluene; acetonitrile; mineral oil; pentane; 1.2: Aldol condensation / 11.3: Suzuki coupling;
DOI:10.1021/ol201426c

Reference yield:

: 1312441-90-9
C₂₉H₄₆O₆

: 1312441-99-8
C₄₅H₆₈O₁₀

Guidance literature:: Multi-step reaction with 11 steps

1.1: tetramethylammonium triacetoxyborohydride / acetic acid; acetonitrile / 4 h / -20 - 25 °C

2.1: pyridinium p-toluenesulfonate / dichloromethane / 2 h / 0 - 25 °C

3.1: diisobutylaluminium hydride / toluene / 1 h / -20 °C

4.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 24 h / 25 °C

5.1: pyridinium p-toluenesulfonate / methanol; chloroform / 48 h / 25 °C

6.1: sodium hydride / tetrahydrofuran; mineral oil / 0.33 h / 0 °C

6.2: 6 h / 25 °C

7.1: tert.-butyl lithium / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; pentane / 0.08 h / -78 °C

7.2: 1 h / -78 °C

8.1: manganese(IV) oxide / dichloromethane / 8 h / 25 °C

9.1: 4-toluenesulfonyl azide; potassium carbonate / acetonitrile / 2 h / 25 °C

9.2: 18 h / 25 °C

10.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C

10.2: 0.5 h / -78 - 25 °C

10.3: 3 h / Reflux

11.1: hydrogen / ethanol / 40 h / 50 °C

With manganese(IV) oxide; 4-toluenesulfonyl azide; hydrogen; tert.-butyl lithium; sodium hexamethyldisilazane; pyridinium p-toluenesulfonate; sodium hydride; diisobutylaluminium hydride; potassium carbonate; N-ethyl-N,N-diisopropylamine; tetramethylammonium triacetoxyborohydride; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol; dichloromethane; chloroform; acetic acid; toluene; acetonitrile; mineral oil; pentane; 10.3: Suzuki coupling;
DOI:10.1021/ol201426c