cis-2,6-dimethyl-α,α-diphenyl-1-piperidinebutanol

Base Information

Chemical Name:cis-2,6-dimethyl-α,α-diphenyl-1-piperidinebutanol
CAS No.:63645-09-0
Molecular Formula:C₂₃H₃₁NO
Molecular Weight:337.505
Hs Code.:

Synonyms:cis-2,6-dimethyl-α,α-diphenyl-1-piperidinebutanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cis-2,6-dimethyl-α,α-diphenyl-1-piperidinebutanol

Chemical Property:

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Technology Process of cis-2,6-dimethyl-α,α-diphenyl-1-piperidinebutanol

There total 5 articles about cis-2,6-dimethyl-α,α-diphenyl-1-piperidinebutanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 63645-07-8
4-(2,6-dimethyl-1-piperidinyl)-1-phenyl-1-butanone

: 591-51-5
phenyllithium

: 63645-09-0
cis-2,6-dimethyl-α,α-diphenyl-1-piperidinebutanol

Guidance literature:: In tetrahydrofuran; diethyl ether; benzene; for 0.75h;
DOI:10.1021/jm00105a003

Reference yield:

: 63645-14-7
methyl 4-(2,6-dimethyl-1-piperidinyl)butanoate

: 63645-09-0
cis-2,6-dimethyl-α,α-diphenyl-1-piperidinebutanol

Guidance literature:: With phenyllithium; In benzene diethyl ether; water;

Reference yield:

: 3308-98-3
2-(3-chloropropyl)-2-phenyl-[1,3]dioxolane

: 63645-09-0
cis-2,6-dimethyl-α,α-diphenyl-1-piperidinebutanol

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaI, 2.) aq. HCl / 1.) reflux, 48 h, 2.) from 80 deg C to RT, 16 h

2: 62 percent / tetrahydrofuran; benzene; diethyl ether / 0.75 h

With hydrogenchloride; sodium iodide; In tetrahydrofuran; diethyl ether; benzene;
DOI:10.1021/jm00105a003