4-Benzyloxy-3-methoxyphenol

Base Information

• Chemical Name: 4-Benzyloxy-3-methoxyphenol
• CAS No.: 40232-88-0
• Molecular Formula: C14H14 O3
• Molecular Weight: 230.263
• Hs Code.: 2909500000
• Mol file: 40232-88-0.mol

Synonyms:Phenol,4-(benzyloxy)-3-methoxy- (6CI); 3-Methoxy-4-benzyloxyphenol;4-Benzyloxy-3-methoxyphenol

Chemical Property of 4-Benzyloxy-3-methoxyphenol

Chemical Property:

• Vapor Pressure: 1.15E-06mmHg at 25°C
• Melting Point: 76-78°C
• Refractive Index: 1.586
• Boiling Point: 390.7°C at 760 mmHg
• PKA: 9.95±0.20(Predicted)
• Flash Point: 190.1°C
• PSA: 38.69000
• Density: 1.171g/cm³
• LogP: 2.97980
• Storage Temp.: Refrigerator
• Solubility.: Chloroform(Slightly), Methanol (Slightly)

Purity/Quality:

HPLC≥98% ^*data from raw suppliers

4-Benzyloxy-3-methoxyphenol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-Benzyloxy-3-methoxyphenol

There total 10 articles about 4-Benzyloxy-3-methoxyphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

4-(benzyloxy)-3-methoxyphenyl formate (868856-34-2) → 4-benzyloxy-3-methoxyphenol (40232-88-0)

Guidance literature:

With water; potassium carbonate; In methanol; at 20 ℃; for 0.5h; Inert atmosphere;

DOI:10.1002/hlca.201000306

Reference yield: 92.0%

3-methoxy-4-(phenylmethoxy)benzaldehyde (2426-87-1) → 4-benzyloxy-3-methoxyphenol (40232-88-0)

Guidance literature:

3-methoxy-4-(phenylmethoxy)benzaldehyde; With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 12h;

With sodium hydroxide; In methanol; water; for 3h; Further stages.;

DOI:10.1016/j.tetlet.2007.01.117

Reference yield:

vanillin (121-33-5,8014-42-4) → 4-benzyloxy-3-methoxyphenol (40232-88-0)

Guidance literature:

Multi-step reaction with 2 steps

1.1: 98 percent / K₂CO₃ / acetone / 5 h / Heating

2.1: m-CPBA / CH₂Cl₂ / 12 h

2.2: 92 percent / NaOH / methanol; H₂O / 3 h

With potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; acetone;

DOI:10.1016/j.tetlet.2007.01.117

upstream raw materials:

3-methoxy-4-(phenylmethoxy)benzaldehyde

4-(benzyloxy)-3-methoxyphenyl formate

benzyl bromide

vanillin

Downstream raw materials:

4-benzyloxy-3-methoxyphenoxyacetic acid

1-(2,4-dihydroxy-5-methoxyphenyl)-2-(4-methoxyphenyl)ethanone

(3S,4R)-4-(4-fluorophenyl)-3-(3-methoxy-4-benzyloxyphenoxymethyl)-1-methylpiperidine

C₁₇H₁₈O₃

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