Technology Process of C24H25F4NO4
There total 9 articles about C24H25F4NO4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium hexamethyldisilazane;
In
N,N-dimethyl-formamide;
at 0 ℃;
DOI:10.3987/COM-08-11407
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate / acetonitrile / Reflux
2: lithium hexamethyldisilazane / N,N-dimethyl-formamide / 0 °C
With
potassium carbonate; lithium hexamethyldisilazane;
In
N,N-dimethyl-formamide; acetonitrile;
DOI:10.3987/COM-08-11407
- Guidance literature:
-
Multi-step reaction with 8 steps
1: triethylsilane / dichloromethane / 20 °C
2: titanium(IV) tetraethanolate / 80 °C
3: titanium tetrachloride / dichloromethane / -78 - 20 °C
4: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 20 °C
5: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 20 °C
6: boron tribromide / dichloromethane / -78 °C
7: potassium carbonate / acetonitrile / Reflux
8: lithium hexamethyldisilazane / N,N-dimethyl-formamide / 0 °C
With
triethylsilane; titanium(IV) tetraethanolate; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; boron tribromide; titanium tetrachloride; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; lithium hexamethyldisilazane;
In
dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol;
4: Kraus oxidation;
DOI:10.3987/COM-08-11407
