7-acetyl-10a-(4-chlorophenyl)-2,3,10,10a-tetrahydro-1H,5H-imidazo[1,2-a]pyrrolo[1,2-d]pyrazin-5-one

Base Information

Chemical Name:7-acetyl-10a-(4-chlorophenyl)-2,3,10,10a-tetrahydro-1H,5H-imidazo[1,2-a]pyrrolo[1,2-d]pyrazin-5-one
CAS No.:1323076-49-8
Molecular Formula:C₁₇H₁₆ClN₃O₂
Molecular Weight:329.786
Hs Code.:

Synonyms:7-acetyl-10a-(4-chlorophenyl)-2,3,10,10a-tetrahydro-1H,5H-imidazo[1,2-a]pyrrolo[1,2-d]pyrazin-5-one

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Chemical Property of 7-acetyl-10a-(4-chlorophenyl)-2,3,10,10a-tetrahydro-1H,5H-imidazo[1,2-a]pyrrolo[1,2-d]pyrazin-5-one

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Technology Process of 7-acetyl-10a-(4-chlorophenyl)-2,3,10,10a-tetrahydro-1H,5H-imidazo[1,2-a]pyrrolo[1,2-d]pyrazin-5-one

There total 5 articles about 7-acetyl-10a-(4-chlorophenyl)-2,3,10,10a-tetrahydro-1H,5H-imidazo[1,2-a]pyrrolo[1,2-d]pyrazin-5-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 1323076-42-1
10a-(4-chlorophenyl)-2,3,10,10a-tetrahydro-1H,5H-imidazo[1,2-a]pyrrolo[1,2-d]pyrazin-5-one

: 75-36-5
acetyl chloride

: 1323076-49-8
7-acetyl-10a-(4-chlorophenyl)-2,3,10,10a-tetrahydro-1H,5H-imidazo[1,2-a]pyrrolo[1,2-d]pyrazin-5-one

: 1323076-48-7
C₁₉H₁₈ClN₃O₃

Guidance literature:: With aluminum (III) chloride; In 1,2-dichloro-ethane; at 20 - 60 ℃; for 24h;

Reference yield:

: 86289-14-7
methyl 1-[2-(4-chlorophenyl)-2-oxoethyl]-1H-pyrrole-2-carboxylate

: 1323076-49-8
7-acetyl-10a-(4-chlorophenyl)-2,3,10,10a-tetrahydro-1H,5H-imidazo[1,2-a]pyrrolo[1,2-d]pyrazin-5-one

: 1323076-48-7
C₁₉H₁₈ClN₃O₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: water; lithium hydroxide / tetrahydrofuran / 20 °C

1.2: pH 2

2.1: 1,2-dichloro-ethane / Reflux

3.1: aluminum (III) chloride / 1,2-dichloro-ethane / 24 h / 20 - 60 °C

With aluminum (III) chloride; water; lithium hydroxide; In tetrahydrofuran; 1,2-dichloro-ethane;

Reference yield:

: 1323076-40-9
1-[2-(4-chlorophenyl)-2-oxoethyl]-1H-pyrrole-2-carboxylic acid

: 1323076-49-8
7-acetyl-10a-(4-chlorophenyl)-2,3,10,10a-tetrahydro-1H,5H-imidazo[1,2-a]pyrrolo[1,2-d]pyrazin-5-one

: 1323076-48-7
C₁₉H₁₈ClN₃O₃

Guidance literature:: Multi-step reaction with 2 steps

1: 1,2-dichloro-ethane / Reflux

2: aluminum (III) chloride / 1,2-dichloro-ethane / 24 h / 20 - 60 °C

With aluminum (III) chloride; In 1,2-dichloro-ethane;