N-((4,5-dihydroxy-9,10-dioxo-9,10-dihydroanthracen-2-yl)methyl)-N,N-dimethylbenzenaminium chloride

Base Information

• Chemical Name: N-((4,5-dihydroxy-9,10-dioxo-9,10-dihydroanthracen-2-yl)methyl)-N,N-dimethylbenzenaminium chloride
• CAS No.: 1425441-21-9
• Molecular Formula: C₂₃H₂₀NO₄*Cl
• Molecular Weight: 409.869
• Mol file: 1425441-21-9.mol

Synonyms:N-((4,5-dihydroxy-9,10-dioxo-9,10-dihydroanthracen-2-yl)methyl)-N,N-dimethylbenzenaminium chloride

Chemical Property of N-((4,5-dihydroxy-9,10-dioxo-9,10-dihydroanthracen-2-yl)methyl)-N,N-dimethylbenzenaminium chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-((4,5-dihydroxy-9,10-dioxo-9,10-dihydroanthracen-2-yl)methyl)-N,N-dimethylbenzenaminium chloride

There total 3 articles about N-((4,5-dihydroxy-9,10-dioxo-9,10-dihydroanthracen-2-yl)methyl)-N,N-dimethylbenzenaminium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

3-(chloromethyl)-1,8-dihydroxyanthracene-9,10-dione (75694-01-8) + N,N-dimethyl-aniline (121-69-7,77733-26-7) → N-((4,5-dihydroxy-9,10-dioxo-9,10-dihydroanthracen-2-yl)methyl)-N,N-dimethylbenzenaminium chloride (1425441-21-9)

Guidance literature:

In chloroform; at 20 ℃; for 336h;

DOI:10.1016/j.bmc.2013.01.015

Reference yield:

1,8-dihydroxy-3-hydroxymethyl-9,10-anthracenedione (481-72-1) → N-((4,5-dihydroxy-9,10-dioxo-9,10-dihydroanthracen-2-yl)methyl)-N,N-dimethylbenzenaminium chloride (1425441-21-9)

Guidance literature:

Multi-step reaction with 2 steps

1: thionyl chloride; N,N-dimethyl-formamide / 26 h / 20 °C

2: chloroform / 336 h / 20 °C

With thionyl chloride; N,N-dimethyl-formamide; In chloroform;

DOI:10.1016/j.bmc.2013.01.015

Reference yield:

4,5-dihydroxy-9,10-dioxo-9,10-dihydroanthracene-2-carbaldehyde (154658-30-7) → N-((4,5-dihydroxy-9,10-dioxo-9,10-dihydroanthracen-2-yl)methyl)-N,N-dimethylbenzenaminium chloride (1425441-21-9)

Guidance literature:

Multi-step reaction with 2 steps

1: thionyl chloride / N,N-dimethyl-formamide / 26 h / 20 °C

2: chloroform / 20 °C

With thionyl chloride; In chloroform; N,N-dimethyl-formamide;

DOI:10.1016/j.ejmech.2014.01.058

upstream raw materials:

3-(chloromethyl)-1,8-dihydroxyanthracene-9,10-dione

N,N-dimethyl-aniline

1,8-dihydroxy-3-hydroxymethyl-9,10-anthracenedione

4,5-dihydroxy-9,10-dioxo-9,10-dihydroanthracene-2-carbaldehyde