C₄₃H₄₈ClN₃O₁₃

Base Information

Chemical Name:C₄₃H₄₈ClN₃O₁₃
CAS No.:1312610-62-0
Molecular Formula:C₄₃H₄₈ClN₃O₁₃
Molecular Weight:850.319
Hs Code.:

C<sub>43</sub>H<sub>48</sub>ClN<sub>3</sub>O<sub>13</sub>

Synonyms:C₄₃H₄₈ClN₃O₁₃

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Chemical Property of C₄₃H₄₈ClN₃O₁₃

Chemical Property:

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Technology Process of C₄₃H₄₈ClN₃O₁₃

There total 10 articles about C₄₃H₄₈ClN₃O₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 15761-39-4,59433-50-0
1-(tert-butoxycarbonyl)-L-proline

: 1312610-61-9
C₂₃H₁₆Br₂ClNO₅

: 1312610-62-0
C₄₃H₄₈ClN₃O₁₃

Guidance literature:: With DMA; In tetrahydrofuran; at 20 ℃;

Reference yield:

: 126463-85-2
4-acetylamino-5-chloro-2-methoxy-3-nitro-benzoic acid methyl ester

: 1312610-62-0
C₄₃H₄₈ClN₃O₁₃

Guidance literature:: Multi-step reaction with 9 steps

1.1: sulfuric acid / methanol / 7 h / Reflux

2.1: copper(I) bromide; tert.-butylnitrite / acetonitrile / 4 h / 70 °C

3.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol / 80 °C / Inert atmosphere

4.1: boron tribromide / dichloromethane / 2 h / -70 - -60 °C

4.2: Cooling with ice

5.1: potassium carbonate / N,N-dimethyl-formamide / 40 °C

6.1: water; lithium hydroxide monohydrate / tetrahydrofuran / 20 °C

7.1: thionyl chloride / 2 h / Reflux

8.1: dichloromethane; diethyl ether / 1 h / -5 - 20 °C

8.2: -5 - 20 °C

9.1: DMA / tetrahydrofuran / 20 °C

With thionyl chloride; tert.-butylnitrite; lithium hydroxide monohydrate; sulfuric acid; water; boron tribromide; sodium carbonate; potassium carbonate; copper(I) bromide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile; 3.1: Suzuki Coupling;

Reference yield:

: 457947-61-4
4-amino-5-chloro-2-methoxy-3-nitro-benzoic acid methyl ester

: 1312610-62-0
C₄₃H₄₈ClN₃O₁₃

Guidance literature:: Multi-step reaction with 8 steps

1.1: copper(I) bromide; tert.-butylnitrite / acetonitrile / 4 h / 70 °C

2.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol / 80 °C / Inert atmosphere

3.1: boron tribromide / dichloromethane / 2 h / -70 - -60 °C

3.2: Cooling with ice

4.1: potassium carbonate / N,N-dimethyl-formamide / 40 °C

5.1: water; lithium hydroxide monohydrate / tetrahydrofuran / 20 °C

6.1: thionyl chloride / 2 h / Reflux

7.1: dichloromethane; diethyl ether / 1 h / -5 - 20 °C

7.2: -5 - 20 °C

8.1: DMA / tetrahydrofuran / 20 °C

With thionyl chloride; tert.-butylnitrite; lithium hydroxide monohydrate; water; boron tribromide; sodium carbonate; potassium carbonate; copper(I) bromide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile; 2.1: Suzuki Coupling;