C₁₄H₁₁ClN₂O₂

Base Information

Chemical Name:C₁₄H₁₁ClN₂O₂
CAS No.:1355227-79-0
Molecular Formula:C₁₄H₁₁ClN₂O₂
Molecular Weight:274.707
Hs Code.:

C<sub>14</sub>H<sub>11</sub>ClN<sub>2</sub>O<sub>2</sub>

Synonyms:C₁₄H₁₁ClN₂O₂

Suppliers and Price of C₁₄H₁₁ClN₂O₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₁₄H₁₁ClN₂O₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₁₄H₁₁ClN₂O₂

There total 6 articles about C₁₄H₁₁ClN₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1355227-77-8
(2E)-3-[4-(4-methoxyphenyl)pyrimidin-5-yl]prop-2-enoic acid

: 1355227-79-0
C₁₄H₁₁ClN₂O₂

Guidance literature:: With oxalyl dichloride; N,N-dimethyl-formamide; In tetrahydrofuran; at 20 ℃; for 3h;

Reference yield:

: 1355227-74-5
ethyl 4-(4-methoxyphenyl)-2-(methylsulfanyl)pyrimidine-5-carboxylate

: 1355227-79-0
C₁₄H₁₁ClN₂O₂

Guidance literature:: Multi-step reaction with 6 steps

1: diisobutylaluminium hydride / toluene / 1.5 h / -78 °C

2: Raney Nickel / ethanol / 2 h / Reflux

3: manganese(IV) oxide / tetrahydrofuran / 20 °C

4: sodium hydride / mineral oil; N,N-dimethyl-formamide / 1 h / Cooling with ice

5: water; lithium hydroxide monohydrate / tetrahydrofuran; ethanol / 0.5 h / 20 °C

6: N,N-dimethyl-formamide; oxalyl dichloride / tetrahydrofuran / 3 h / 20 °C

With manganese(IV) oxide; oxalyl dichloride; lithium hydroxide monohydrate; water; sodium hydride; diisobutylaluminium hydride; N,N-dimethyl-formamide; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide; toluene; mineral oil;

Reference yield:

: 1355227-76-7
[4-(4-methoxyphenyl)-2-(methylsulfanyl)pyrimidin-5-yl]methanol

: 1355227-79-0
C₁₄H₁₁ClN₂O₂

Guidance literature:: Multi-step reaction with 5 steps

1: Raney Nickel / ethanol / 2 h / Reflux

2: manganese(IV) oxide / tetrahydrofuran / 20 °C

3: sodium hydride / mineral oil; N,N-dimethyl-formamide / 1 h / Cooling with ice

4: water; lithium hydroxide monohydrate / tetrahydrofuran; ethanol / 0.5 h / 20 °C

5: N,N-dimethyl-formamide; oxalyl dichloride / tetrahydrofuran / 3 h / 20 °C

With manganese(IV) oxide; oxalyl dichloride; lithium hydroxide monohydrate; water; sodium hydride; N,N-dimethyl-formamide; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide; mineral oil;