C₂₇H₃₄FNO₄SSi

Base Information

Chemical Name:C₂₇H₃₄FNO₄SSi
CAS No.:1374233-28-9
Molecular Formula:C₂₇H₃₄FNO₄SSi
Molecular Weight:515.721
Hs Code.:

C<sub>27</sub>H<sub>34</sub>FNO<sub>4</sub>SSi

Synonyms:C₂₇H₃₄FNO₄SSi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₇H₃₄FNO₄SSi

Chemical Property:

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Technology Process of C₂₇H₃₄FNO₄SSi

There total 9 articles about C₂₇H₃₄FNO₄SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 766-98-3
1-ethynyl-4-fluorobenzene

: 1374233-27-8
C₁₉H₃₀BrNO₄SSi

: 1374233-28-9
C₂₇H₃₄FNO₄SSi

Guidance literature:: With piperidine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tri-tert-butyl phosphine; In N,N-dimethyl-formamide; at 80 ℃; Inert atmosphere;

Reference yield:

: 59557-92-5
2-bromo-5-methoxyaniline

: 1374233-28-9
C₂₇H₃₄FNO₄SSi

Guidance literature:: Multi-step reaction with 8 steps

1.1: pyridine / dichloromethane / 0.5 h / 0 - 20 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 80 °C

3.1: triethylamine; lithium chloride / palladium diacetate; triphenylphosphine / N,N-dimethyl-formamide / 1.5 h / 120 °C / Inert atmosphere

4.1: diethylzinc / hexane; toluene / 0 - 20 °C

5.1: N-Bromosuccinimide / dichloromethane / 24 h / 0 - 20 °C

6.1: boron tribromide / dichloromethane / 0.33 h / 0 °C

6.2: Cooling with ice

7.1: triethylamine / dmap / tetrahydrofuran / 1.5 h / 0 - 20 °C

8.1: piperidine / bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tri-tert-butyl phosphine / N,N-dimethyl-formamide / 80 °C / Inert atmosphere

With piperidine; pyridine; N-Bromosuccinimide; diethylzinc; boron tribromide; potassium carbonate; triethylamine; lithium chloride; dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tri-tert-butyl phosphine; palladium diacetate; triphenylphosphine; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; toluene;

Reference yield:

: 5344-78-5
4-bromo-3-nitroanizole

: 1374233-28-9
C₂₇H₃₄FNO₄SSi

Guidance literature:: Multi-step reaction with 9 steps

1.1: acetic acid; zinc / ethanol / 20 °C

2.1: pyridine / dichloromethane / 0.5 h / 0 - 20 °C

3.1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 80 °C

4.1: triethylamine; lithium chloride / palladium diacetate; triphenylphosphine / N,N-dimethyl-formamide / 1.5 h / 120 °C / Inert atmosphere

5.1: diethylzinc / hexane; toluene / 0 - 20 °C

6.1: N-Bromosuccinimide / dichloromethane / 24 h / 0 - 20 °C

7.1: boron tribromide / dichloromethane / 0.33 h / 0 °C

7.2: Cooling with ice

8.1: triethylamine / dmap / tetrahydrofuran / 1.5 h / 0 - 20 °C

9.1: piperidine / bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tri-tert-butyl phosphine / N,N-dimethyl-formamide / 80 °C / Inert atmosphere

With piperidine; pyridine; N-Bromosuccinimide; diethylzinc; boron tribromide; potassium carbonate; acetic acid; triethylamine; lithium chloride; zinc; dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tri-tert-butyl phosphine; palladium diacetate; triphenylphosphine; In tetrahydrofuran; ethanol; hexane; dichloromethane; N,N-dimethyl-formamide; toluene;