4-ethoxycarbonyl-2-(2-phenylquinolin-4-yl)pyridine N-oxide

Base Information

Chemical Name:4-ethoxycarbonyl-2-(2-phenylquinolin-4-yl)pyridine N-oxide
CAS No.:1286763-45-8
Molecular Formula:C₂₃H₁₈N₂O₃
Molecular Weight:370.408
Hs Code.:

Synonyms:4-ethoxycarbonyl-2-(2-phenylquinolin-4-yl)pyridine N-oxide

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Chemical Property of 4-ethoxycarbonyl-2-(2-phenylquinolin-4-yl)pyridine N-oxide

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Technology Process of 4-ethoxycarbonyl-2-(2-phenylquinolin-4-yl)pyridine N-oxide

There total 2 articles about 4-ethoxycarbonyl-2-(2-phenylquinolin-4-yl)pyridine N-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 14906-37-7
ethyl isonicotinate N-oxide

: 4979-79-7
4-chloro-2-phenylquinoline

: 1286763-45-8
4-ethoxycarbonyl-2-(2-phenylquinolin-4-yl)pyridine N-oxide

Guidance literature:: With tri-tert-butyl phosphine; palladium diacetate; potassium carbonate; In toluene; at 120 ℃; for 24h; Inert atmosphere;
DOI:10.1021/ol200565u

Reference yield:

: 1570-45-2
isonicotinic acid ethylester

: 1286763-45-8
4-ethoxycarbonyl-2-(2-phenylquinolin-4-yl)pyridine N-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: dihydrogen peroxide / acetic acid / 70 °C / Inert atmosphere

2: tri-tert-butyl phosphine; palladium diacetate; potassium carbonate / toluene / 24 h / 120 °C / Inert atmosphere

With tri-tert-butyl phosphine; dihydrogen peroxide; palladium diacetate; potassium carbonate; In acetic acid; toluene;
DOI:10.1021/ol200565u