(S)-octanedioic acid benzyloxyamide (2-phenyl-1-phenylcarbamoyl-ethyl)amide

Base Information

Chemical Name:(S)-octanedioic acid benzyloxyamide (2-phenyl-1-phenylcarbamoyl-ethyl)amide
CAS No.:449728-85-2
Molecular Formula:C₃₀H₃₅N₃O₄
Molecular Weight:501.626
Hs Code.:

Synonyms:(S)-octanedioic acid benzyloxyamide (2-phenyl-1-phenylcarbamoyl-ethyl)amide

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Chemical Property of (S)-octanedioic acid benzyloxyamide (2-phenyl-1-phenylcarbamoyl-ethyl)amide

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Technology Process of (S)-octanedioic acid benzyloxyamide (2-phenyl-1-phenylcarbamoyl-ethyl)amide

There total 5 articles about (S)-octanedioic acid benzyloxyamide (2-phenyl-1-phenylcarbamoyl-ethyl)amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3946-32-5
suberic acid monomethyl ester

: 449728-85-2
(S)-octanedioic acid benzyloxyamide (2-phenyl-1-phenylcarbamoyl-ethyl)amide

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / iPr₂NEt; BOP-Cl / CH₂Cl₂

2: 68 percent / aq. LiOH / tetrahydrofuran / 20 °C

3: NMM / tetrahydrofuran

4: 160 mg / NMM / tetrahydrofuran / 2.25 h

With 4-methyl-morpholine; lithium hydroxide; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm0208119

Reference yield:

: 2687-43-6
O-benzylhydoxylamine hydrochloride

: 449728-85-2
(S)-octanedioic acid benzyloxyamide (2-phenyl-1-phenylcarbamoyl-ethyl)amide

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / iPr₂NEt; BOP-Cl / CH₂Cl₂

2: 68 percent / aq. LiOH / tetrahydrofuran / 20 °C

3: NMM / tetrahydrofuran

4: 160 mg / NMM / tetrahydrofuran / 2.25 h

With 4-methyl-morpholine; lithium hydroxide; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm0208119

Reference yield:

: 251304-81-1
8-((benzyloxy)amino)-8-oxooctanoic acid

: 449728-85-2
(S)-octanedioic acid benzyloxyamide (2-phenyl-1-phenylcarbamoyl-ethyl)amide

Guidance literature:: Multi-step reaction with 2 steps

1: NMM / tetrahydrofuran

2: 160 mg / NMM / tetrahydrofuran / 2.25 h

With 4-methyl-morpholine; In tetrahydrofuran;
DOI:10.1021/jm0208119