4-(4-(1-hydroxy-4-oxocyclohexa-2,5-dienyl)-1H-1,2,3-triazol-1-yl)benzimidamide

Base Information

Chemical Name:4-(4-(1-hydroxy-4-oxocyclohexa-2,5-dienyl)-1H-1,2,3-triazol-1-yl)benzimidamide
CAS No.:1361574-72-2
Molecular Formula:C₁₅H₁₃N₅O₂
Molecular Weight:295.301
Hs Code.:

Synonyms:4-(4-(1-hydroxy-4-oxocyclohexa-2,5-dienyl)-1H-1,2,3-triazol-1-yl)benzimidamide

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Chemical Property of 4-(4-(1-hydroxy-4-oxocyclohexa-2,5-dienyl)-1H-1,2,3-triazol-1-yl)benzimidamide

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Technology Process of 4-(4-(1-hydroxy-4-oxocyclohexa-2,5-dienyl)-1H-1,2,3-triazol-1-yl)benzimidamide

There total 3 articles about 4-(4-(1-hydroxy-4-oxocyclohexa-2,5-dienyl)-1H-1,2,3-triazol-1-yl)benzimidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 4.0%

: 935684-39-2
4-ethynyl-4-hydroxycyclohexa-2,5-dien-1-one

: 1361574-71-1
4-azidobenzimidamide sulfate

: 1361574-72-2
4-(4-(1-hydroxy-4-oxocyclohexa-2,5-dienyl)-1H-1,2,3-triazol-1-yl)benzimidamide

Guidance literature:: With 2,6-dimethylpyridine; copper(l) iodide; In acetonitrile; at 0 ℃; for 18h; Inert atmosphere;
DOI:10.1016/j.bmc.2011.12.018

Reference yield:

: 150-76-5
4-methoxy-phenol

: 1361574-72-2
4-(4-(1-hydroxy-4-oxocyclohexa-2,5-dienyl)-1H-1,2,3-triazol-1-yl)benzimidamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: [bis(acetoxy)iodo]benzene / 1.66 h / Inert atmosphere

2.1: tetrahydrofuran / -78 - 20 °C / Inert atmosphere

2.2: Saturated solution

3.1: 2,6-dimethylpyridine; copper(l) iodide / acetonitrile / 18 h / 0 °C / Inert atmosphere

With 2,6-dimethylpyridine; copper(l) iodide; [bis(acetoxy)iodo]benzene; In tetrahydrofuran; acetonitrile;
DOI:10.1016/j.bmc.2011.12.018

Reference yield:

: 935-50-2
4,4-dimethoxycyclohexa-2,5-dienone

: 1361574-72-2
4-(4-(1-hydroxy-4-oxocyclohexa-2,5-dienyl)-1H-1,2,3-triazol-1-yl)benzimidamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrahydrofuran / -78 - 20 °C / Inert atmosphere

1.2: Saturated solution

2.1: 2,6-dimethylpyridine; copper(l) iodide / acetonitrile / 18 h / 0 °C / Inert atmosphere

With 2,6-dimethylpyridine; copper(l) iodide; In tetrahydrofuran; acetonitrile;
DOI:10.1016/j.bmc.2011.12.018