(8-(methoxyimino)-5,6,7,8-tetrahydronaphthalen-1-yl)(3-nitrophenyl)methanone

Base Information

Chemical Name:(8-(methoxyimino)-5,6,7,8-tetrahydronaphthalen-1-yl)(3-nitrophenyl)methanone
CAS No.:1417412-42-0
Molecular Formula:C₁₈H₁₆N₂O₄
Molecular Weight:324.336
Hs Code.:

Synonyms:(8-(methoxyimino)-5,6,7,8-tetrahydronaphthalen-1-yl)(3-nitrophenyl)methanone

Suppliers and Price of (8-(methoxyimino)-5,6,7,8-tetrahydronaphthalen-1-yl)(3-nitrophenyl)methanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (8-(methoxyimino)-5,6,7,8-tetrahydronaphthalen-1-yl)(3-nitrophenyl)methanone

Chemical Property:

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Technology Process of (8-(methoxyimino)-5,6,7,8-tetrahydronaphthalen-1-yl)(3-nitrophenyl)methanone

There total 2 articles about (8-(methoxyimino)-5,6,7,8-tetrahydronaphthalen-1-yl)(3-nitrophenyl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 6330-40-1
2-(3-nitrophenyl)-2-oxoacetic acid

: 104354-39-4,192461-77-1
3,4-dihydro-naphthalen-1(2H)-one oxime O-methyl ether

: 1417412-42-0
(8-(methoxyimino)-5,6,7,8-tetrahydronaphthalen-1-yl)(3-nitrophenyl)methanone

Guidance literature:: With ammonium peroxodisulfate; palladium diacetate; In diethylene glycol dimethyl ether; at 70 ℃; for 7h; Sealed tube;
DOI:10.1039/c2cc38433g

Reference yield:

: 121-89-1
3-Nitroacetophenone

: 1417412-42-0
(8-(methoxyimino)-5,6,7,8-tetrahydronaphthalen-1-yl)(3-nitrophenyl)methanone

Guidance literature:: Multi-step reaction with 2 steps

1: selenium(IV) oxide; pyridine

2: palladium diacetate; ammonium peroxodisulfate / diethylene glycol dimethyl ether / 7 h / 70 °C / Sealed tube

With pyridine; selenium(IV) oxide; ammonium peroxodisulfate; palladium diacetate; In diethylene glycol dimethyl ether;
DOI:10.1039/c2cc38433g