acide α,α'-di-O-hydroxyphenoxy sebacique

Base Information

Chemical Name:acide α,α'-di-O-hydroxyphenoxy sebacique
CAS No.:128312-46-9
Molecular Formula:C₂₂H₂₆O₈
Molecular Weight:418.444
Hs Code.:

Synonyms:acide α,α'-di-O-hydroxyphenoxy sebacique

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of acide α,α'-di-O-hydroxyphenoxy sebacique

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Technology Process of acide α,α'-di-O-hydroxyphenoxy sebacique

There total 6 articles about acide α,α'-di-O-hydroxyphenoxy sebacique which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 128312-42-5
acide α,α'-di-O-methoxyphenoxy sebacique

: 128312-46-9
acide α,α'-di-O-hydroxyphenoxy sebacique

Guidance literature:: With boron tribromide; In dichloromethane; at 17 - 18 ℃; for 24h;

Reference yield:

: 111-20-6,26776-29-4
1,10-decanedioic acid

: 128312-46-9
acide α,α'-di-O-hydroxyphenoxy sebacique

Guidance literature:: Multi-step reaction with 6 steps

1: thionyl chloride

2: bromine / 2 h / Heating

3: Ambient temperature

4: 82 percent / K₂CO₃, tris(3,6-dioxaheptyl)amine / toluene / 14 h / 75 °C

5: 53 percent / KOH / H₂O / 45 h / Heating

6: 32 percent / BBr₃ / CH₂Cl₂ / 24 h / 17 - 18 °C

With potassium hydroxide; thionyl chloride; Tris(3,6-dioxaheptyl)amine; bromine; boron tribromide; potassium carbonate; In dichloromethane; water; toluene;

Reference yield:

: 111-19-3
sebacoyl chloride

: 128312-46-9
acide α,α'-di-O-hydroxyphenoxy sebacique

Guidance literature:: Multi-step reaction with 5 steps

1: bromine / 2 h / Heating

2: Ambient temperature

3: 82 percent / K₂CO₃, tris(3,6-dioxaheptyl)amine / toluene / 14 h / 75 °C

4: 53 percent / KOH / H₂O / 45 h / Heating

5: 32 percent / BBr₃ / CH₂Cl₂ / 24 h / 17 - 18 °C

With potassium hydroxide; Tris(3,6-dioxaheptyl)amine; bromine; boron tribromide; potassium carbonate; In dichloromethane; water; toluene;