1-C₆H₅CONHCH₂-1,2-dicarba-closo-dodecaborane⁽¹²⁾

Base Information

Chemical Name:1-C₆H₅CONHCH₂-1,2-dicarba-closo-dodecaborane⁽¹²⁾
CAS No.:224790-08-3
Molecular Formula:C₁₀H₁₉B₁₀NO
Molecular Weight:277.377
Hs Code.:

1-C<sub>6</sub>H<sub>5</sub>CONHCH<sub>2</sub>-1,2-dicarba-closo-dodecaborane<sup>(12)</sup>

Synonyms:1-C₆H₅CONHCH₂-1,2-dicarba-closo-dodecaborane⁽¹²⁾

Suppliers and Price of 1-C₆H₅CONHCH₂-1,2-dicarba-closo-dodecaborane⁽¹²⁾

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-C₆H₅CONHCH₂-1,2-dicarba-closo-dodecaborane⁽¹²⁾

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Technology Process of 1-C₆H₅CONHCH₂-1,2-dicarba-closo-dodecaborane⁽¹²⁾

There total 4 articles about 1-C₆H₅CONHCH₂-1,2-dicarba-closo-dodecaborane⁽¹²⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 591-50-4
iodobenzene

: 140662-84-6
1-aminomethyl-1,2-dicarba-closo-dodecaborane⁽¹²⁾ hydrochloride

: 201230-82-2
carbon monoxide

: 224790-08-3
1-C₆H₅CONHCH₂-1,2-dicarba-closo-dodecaborane⁽¹²⁾

Guidance literature:: With multi-walled carbon nanotubes supported palladium nanoparticles; In toluene; at 130 ℃; for 5h; under 7757.43 Torr; Inert atmosphere;
DOI:10.1016/j.jorganchem.2013.05.014

Reference yield: 76.0%

: 23836-16-0
1-(aminomethyl)-1,2-closo-dicarbadodecaborane⁽¹²⁾

: 65-85-0,8013-63-6
benzoic acid

: 530-62-1
1,1'-carbonyldiimidazole

: 224790-08-3
1-C₆H₅CONHCH₂-1,2-dicarba-closo-dodecaborane⁽¹²⁾

Guidance literature:: With pyridine; In tetrahydrofuran; pyridine; byproducts: C5H5NHCl; N2-atmosphere; stirring carboxylic acid with 1 equiv. carbonyldiimidazole in THF at room temp. for 30 min, addn. of 1 equiv. carborane (in pyridine), stirring overnight; filtration off of pyridinium chloride, evapn. (reduced pressure), dissoln. in CH2Cl2, chromy. (SiO2, AcOEt);
DOI:10.1021/ic981223h

Reference yield: 63.0%

: 108-86-1,52753-63-6
bromobenzene

: 140662-84-6
1-aminomethyl-1,2-dicarba-closo-dodecaborane⁽¹²⁾ hydrochloride

: 201230-82-2
carbon monoxide

: 224790-08-3
1-C₆H₅CONHCH₂-1,2-dicarba-closo-dodecaborane⁽¹²⁾

Guidance literature:: With potassium tert-butylate; In toluene; at 120 ℃; for 5h; under 6205.94 Torr; Inert atmosphere;
DOI:10.1002/pola.26829