(+/-)-N-tert-butoxycarbonyl-5-(tert-butyldiphenylsilyloxy)-3-piperidene

Base Information

Chemical Name:(+/-)-N-tert-butoxycarbonyl-5-(tert-butyldiphenylsilyloxy)-3-piperidene
CAS No.:1001919-23-8
Molecular Formula:C₂₆H₃₅NO₃Si
Molecular Weight:437.654
Hs Code.:

Synonyms:(+/-)-N-tert-butoxycarbonyl-5-(tert-butyldiphenylsilyloxy)-3-piperidene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-N-tert-butoxycarbonyl-5-(tert-butyldiphenylsilyloxy)-3-piperidene

Chemical Property:

Purity/Quality:

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Technology Process of (+/-)-N-tert-butoxycarbonyl-5-(tert-butyldiphenylsilyloxy)-3-piperidene

There total 3 articles about (+/-)-N-tert-butoxycarbonyl-5-(tert-butyldiphenylsilyloxy)-3-piperidene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 58479-61-1
tert-butylchlorodiphenylsilane

: 224779-27-5
tert-butyl 3-hydroxy-1,2,3,6-tetrahydropyridine-N-carboxylate

: 1001919-23-8
(+/-)-N-tert-butoxycarbonyl-5-(tert-butyldiphenylsilyloxy)-3-piperidene

Guidance literature:: With 1H-imidazole; dmap; In dichloromethane; at 20 ℃;
DOI:10.1002/adsc.200600559

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1001919-23-8
(+/-)-N-tert-butoxycarbonyl-5-(tert-butyldiphenylsilyloxy)-3-piperidene

Guidance literature:: Multi-step reaction with 3 steps

1.1: H₂O / 6 h / 100 °C

1.2: 66 percent / aq. NaOH / dioxane / 20 °C

2.1: 99 percent / bis(tricyclohexylphosphine)benzylidene Ru(IV) dichloride / CH₂Cl₂ / 20 °C

3.1: 99 percent / imidazole; DMAP / CH₂Cl₂ / 20 °C

With 1H-imidazole; dmap; Grubbs catalyst first generation; In dichloromethane; water;
DOI:10.1002/adsc.200600559

Reference yield:

: 224779-26-4
N-allyl-N-(2-hydroxy-but-3-enyl)-carbamic acid tert-butyl ester

: 1001919-23-8
(+/-)-N-tert-butoxycarbonyl-5-(tert-butyldiphenylsilyloxy)-3-piperidene

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / bis(tricyclohexylphosphine)benzylidene Ru(IV) dichloride / CH₂Cl₂ / 20 °C

2: 99 percent / imidazole; DMAP / CH₂Cl₂ / 20 °C

With 1H-imidazole; dmap; Grubbs catalyst first generation; In dichloromethane;
DOI:10.1002/adsc.200600559