2-(2'-O-benzyl-3',4',6'-tri-O-benzoyl-1-thio-β-D-glucopyranosyl)-benzoxazole

Base Information

Chemical Name:2-(2'-O-benzyl-3',4',6'-tri-O-benzoyl-1-thio-β-D-glucopyranosyl)-benzoxazole
CAS No.:862537-76-6
Molecular Formula:C₄₁H₃₃NO₉S
Molecular Weight:715.78
Hs Code.:

Synonyms:2-(2'-O-benzyl-3',4',6'-tri-O-benzoyl-1-thio-β-D-glucopyranosyl)-benzoxazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(2'-O-benzyl-3',4',6'-tri-O-benzoyl-1-thio-β-D-glucopyranosyl)-benzoxazole

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Technology Process of 2-(2'-O-benzyl-3',4',6'-tri-O-benzoyl-1-thio-β-D-glucopyranosyl)-benzoxazole

There total 1 articles about 2-(2'-O-benzyl-3',4',6'-tri-O-benzoyl-1-thio-β-D-glucopyranosyl)-benzoxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 950902-50-8
(2R,3S,4S,5R,6S)-6-(Benzooxazol-2-ylsulfanyl)-5-benzyloxy-2-hydroxymethyl-tetrahydro-pyran-3,4-diol

: 98-88-4
benzoyl chloride

: 862537-76-6
2-(2'-O-benzyl-3',4',6'-tri-O-benzoyl-1-thio-β-D-glucopyranosyl)-benzoxazole

Guidance literature:: With pyridine; for 1h;
DOI:10.1021/ol050969y

Reference yield: 14.0%

: 862537-76-6
2-(2'-O-benzyl-3',4',6'-tri-O-benzoyl-1-thio-β-D-glucopyranosyl)-benzoxazole

: 4064-06-6
1,2:3,4-di-O-isopropylidene-α-D-galactopyranose

: 6-O-(2'-O-benzyl-3',4',6'-tri-O-benzoyl-α-D-glucopyranosyl)-1,2:3,4-di-O-isopropylidene-α-D-galactopyranoside

Guidance literature:: With 5A molecular sieve; copper(II) bis(trifluoromethanesulfonate); In dichloromethane; at 20 ℃; for 14h;
DOI:10.1021/ol701466u

Reference yield:

: 862537-76-6
2-(2'-O-benzyl-3',4',6'-tri-O-benzoyl-1-thio-β-D-glucopyranosyl)-benzoxazole

: 53008-65-4,641635-63-4
methyl 2,3,4-tri-O-benzyl-D-glucopyranoside

: methyl 2-O-benzyl-3, 4, 6-tri-O-benzoyl-D-glucopyranosyl-β-(1→6)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

: 1233488-82-8
methyl 2-O-benzyl-3, 4, 6-tri-O-benzoyl-D-glucopyranosyl-α-(1→6)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

Guidance literature:: With silver trifluoromethanesulfonate; In 1,2-dichloro-ethane; at 20 ℃; for 1h; optical yield given as %de; stereoselective reaction; Molecular sieve;
DOI:10.1021/ol1023079