chloro-difluoro-thioacetyl fluoride

Base Information

• Chemical Name: chloro-difluoro-thioacetyl fluoride
• CAS No.: 1588-39-2
• Molecular Formula: C₂ClF₃S
• Molecular Weight: 148.536
• Mol file: 1588-39-2.mol

Synonyms:chloro-difluoro-thioacetyl fluoride

Chemical Property of chloro-difluoro-thioacetyl fluoride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of chloro-difluoro-thioacetyl fluoride

There total 2 articles about chloro-difluoro-thioacetyl fluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(Chlordifluormethyl)fluorsulfin (141062-68-2) → Chlorotrifluoroethylene (79-38-9,9036-80-0) + chloro-difluoro-thioacetyl fluoride (1588-39-2)

Guidance literature:

In neat (no solvent); Product distribution; Mechanism; thermolysis (at room temperature), other sulfine;

Reference yield:

2-chlorotetrafluoroethanethiol (812-19-1) → chloro-difluoro-thioacetyl fluoride (1588-39-2) + hydrogen fluoride (7664-39-3,12381-92-9,32057-09-3,74835-82-8)

Guidance literature:

DOI:10.1021/jo01016a008

Reference yield: 79.0%

sodium azide + chloro-difluoro-thioacetyl fluoride (1588-39-2) → chlorodifluoroacetonitrile (421-05-6)

Guidance literature:

In toluene; byproducts: N2; temperature being kept below 40°C during mixing and then raised to 60°C; NaN3 activated by hydrazine hydrate;

upstream raw materials:

(Chlordifluormethyl)fluorsulfin

2-chlorotetrafluoroethanethiol

Downstream raw materials:

chlorodifluoroacetonitrile

Difluorchlordithioessigsaeure-phenylester

sulfur

Refernces