N-(N-benzyloxycarbonyl-L-leucyl)-L-phosphotryptophan diethyl ester

Base Information

Chemical Name:N-(N-benzyloxycarbonyl-L-leucyl)-L-phosphotryptophan diethyl ester
CAS No.:850463-70-6
Molecular Formula:C₂₈H₃₈N₃O₆P
Molecular Weight:543.6
Hs Code.:

Synonyms:N-(N-benzyloxycarbonyl-L-leucyl)-L-phosphotryptophan diethyl ester

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Chemical Property of N-(N-benzyloxycarbonyl-L-leucyl)-L-phosphotryptophan diethyl ester

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Technology Process of N-(N-benzyloxycarbonyl-L-leucyl)-L-phosphotryptophan diethyl ester

There total 1 articles about N-(N-benzyloxycarbonyl-L-leucyl)-L-phosphotryptophan diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 2018-66-8
Z-Leu-OH

: 219922-15-3
(R)-phosphotryptophan diethyl ester

: 850463-70-6
N-(N-benzyloxycarbonyl-L-leucyl)-L-phosphotryptophan diethyl ester

Guidance literature:: With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 21h;
DOI:10.1016/j.ejmech.2004.10.013

Reference yield:

: 850463-70-6
N-(N-benzyloxycarbonyl-L-leucyl)-L-phosphotryptophan diethyl ester

: 850463-66-0
N-[N-(N-benzyloxycarbonyl-L-alanyl)-L-leucyl]-L-phosphotryptophan diethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / ammonium formate / Pd/C / methanol / 3 h / 20 °C

2: 92 percent / DCC; HOBt / dimethylformamide / 21 h / 0 - 20 °C

With ammonium formate; benzotriazol-1-ol; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2004.10.013

Reference yield:

: 850463-70-6
N-(N-benzyloxycarbonyl-L-leucyl)-L-phosphotryptophan diethyl ester

: 850463-67-1
N-[N-(N-benzyloxycarbonyl-D-alanyl)-L-leucyl]-L-phosphotryptophan diethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / ammonium formate / Pd/C / methanol / 3 h / 20 °C

2: 85 percent / DCC; HOBt / dimethylformamide / 21 h / 0 - 20 °C

With ammonium formate; benzotriazol-1-ol; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2004.10.013