(Z)-2-bromo-3-[1-(4-methylphenylsulfonyl)-1H-pyrrol-3-yl]prop-2-en-1-ol

Base Information

Chemical Name:(Z)-2-bromo-3-[1-(4-methylphenylsulfonyl)-1H-pyrrol-3-yl]prop-2-en-1-ol
CAS No.:1342341-43-8
Molecular Formula:C₁₄H₁₄BrNO₃S
Molecular Weight:356.24
Hs Code.:

Synonyms:(Z)-2-bromo-3-[1-(4-methylphenylsulfonyl)-1H-pyrrol-3-yl]prop-2-en-1-ol

Suppliers and Price of (Z)-2-bromo-3-[1-(4-methylphenylsulfonyl)-1H-pyrrol-3-yl]prop-2-en-1-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-2-bromo-3-[1-(4-methylphenylsulfonyl)-1H-pyrrol-3-yl]prop-2-en-1-ol

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Technology Process of (Z)-2-bromo-3-[1-(4-methylphenylsulfonyl)-1H-pyrrol-3-yl]prop-2-en-1-ol

There total 3 articles about (Z)-2-bromo-3-[1-(4-methylphenylsulfonyl)-1H-pyrrol-3-yl]prop-2-en-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1342341-42-7
methyl (Z)-2-bromo-3-[1-(4-methylphenylsulfonyl)-1H-pyrrol-3-yl]prop-2-enoate

: 1342341-43-8
(Z)-2-bromo-3-[1-(4-methylphenylsulfonyl)-1H-pyrrol-3-yl]prop-2-en-1-ol

Guidance literature:: With diisobutylaluminium hydride; In tetrahydrofuran; hexane; Cooling;
DOI:10.1055/s-0030-1260098

Reference yield:

: C₈H₈BrNO₂

: 1342341-43-8
(Z)-2-bromo-3-[1-(4-methylphenylsulfonyl)-1H-pyrrol-3-yl]prop-2-en-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h / 0 °C

1.2: 0.5 h / 0 °C

2.1: diisobutylaluminium hydride / tetrahydrofuran; hexane / Cooling

With sodium hydride; diisobutylaluminium hydride; In tetrahydrofuran; hexane; mineral oil;
DOI:10.1055/s-0030-1260098

Reference yield:

: 7126-39-8
pyrrole-3-carboxaldehyde

: 1342341-43-8
(Z)-2-bromo-3-[1-(4-methylphenylsulfonyl)-1H-pyrrol-3-yl]prop-2-en-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1.1: chloroform / 36 h / 80 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h / 0 °C

2.2: 0.5 h / 0 °C

3.1: diisobutylaluminium hydride / tetrahydrofuran; hexane / Cooling

With sodium hydride; diisobutylaluminium hydride; In tetrahydrofuran; hexane; chloroform; mineral oil;
DOI:10.1055/s-0030-1260098