C₃₃H₅₄N₂O₈

Base Information

• Chemical Name: C₃₃H₅₄N₂O₈
• CAS No.: 1270005-46-3
• Molecular Formula: C₃₃H₅₄N₂O₈
• Molecular Weight: 606.8
• Mol file: 1270005-46-3.mol

Synonyms:C₃₃H₅₄N₂O₈

Chemical Property of C₃₃H₅₄N₂O₈

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₃₃H₅₄N₂O₈

There total 2 articles about C₃₃H₅₄N₂O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

EDTA-tBu4 + benzyl bromide (100-39-0) → C33H54N2O8 (1270005-46-3)

Guidance literature:

With 18-crown-6 ether; potassium carbonate; In 1-methyl-pyrrolidin-2-one; at 60 ℃; for 72h; Inert atmosphere;

DOI:10.1039/c0ob00909a

Reference yield:

bromoacetic acid tert-butyl ester (5292-43-3) → C33H54N2O8 (1270005-46-3)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / acetonitrile / 0 - 20 °C

2: 18-crown-6 ether; potassium carbonate / 1-methyl-pyrrolidin-2-one / 72 h / 60 °C / Inert atmosphere

With 18-crown-6 ether; potassium carbonate; In 1-methyl-pyrrolidin-2-one; acetonitrile; 2: Stevens rearrangement;

DOI:10.1039/c0ob00909a

Reference yield: 100.0%

C33H54N2O8 (1270005-46-3) → benzyl-EDTA (1270005-50-9)

Guidance literature:

With trifluoroacetic acid; at 20 ℃;

DOI:10.1039/c0ob00909a

upstream raw materials:

bromoacetic acid tert-butyl ester

benzyl bromide

Downstream raw materials:

benzyl-EDTA