dimethyl[N-(1,1-dimethylethyl)-1,1-dimethyl-1-[(1,2,3,4,5-η)-3,4-diphenyl-2,4-cyclopentadien-1-yl]silanaminato-(2-)-κ-N]titanium

Base Information

Chemical Name:dimethyl[N-(1,1-dimethylethyl)-1,1-dimethyl-1-[(1,2,3,4,5-η)-3,4-diphenyl-2,4-cyclopentadien-1-yl]silanaminato-(2-)-κ-N]titanium
CAS No.:475995-45-0
Molecular Formula:C₂₅H₃₃NSiTi
Molecular Weight:423.509
Hs Code.:

Synonyms:dimethyl[N-(1,1-dimethylethyl)-1,1-dimethyl-1-[(1,2,3,4,5-η)-3,4-diphenyl-2,4-cyclopentadien-1-yl]silanaminato-(2-)-κ-N]titanium

Suppliers and Price of dimethyl[N-(1,1-dimethylethyl)-1,1-dimethyl-1-[(1,2,3,4,5-η)-3,4-diphenyl-2,4-cyclopentadien-1-yl]silanaminato-(2-)-κ-N]titanium

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of dimethyl[N-(1,1-dimethylethyl)-1,1-dimethyl-1-[(1,2,3,4,5-η)-3,4-diphenyl-2,4-cyclopentadien-1-yl]silanaminato-(2-)-κ-N]titanium

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of dimethyl[N-(1,1-dimethylethyl)-1,1-dimethyl-1-[(1,2,3,4,5-η)-3,4-diphenyl-2,4-cyclopentadien-1-yl]silanaminato-(2-)-κ-N]titanium

There total 1 articles about dimethyl[N-(1,1-dimethylethyl)-1,1-dimethyl-1-[(1,2,3,4,5-η)-3,4-diphenyl-2,4-cyclopentadien-1-yl]silanaminato-(2-)-κ-N]titanium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.5%

: 475995-44-9
dichloro[N-(1,1-dimethylethyl)-1,1-dimethyl-1-[(1,2,3,4,5-η)-3,4-diphenyl-2,4-cyclopentadien-1-yl]silanaminato-(2-)-κ-N]titanium

: 917-54-4
methyllithium

: 475995-45-0
dimethyl[N-(1,1-dimethylethyl)-1,1-dimethyl-1-[(1,2,3,4,5-η)-3,4-diphenyl-2,4-cyclopentadien-1-yl]silanaminato-(2-)-κ-N]titanium

Guidance literature:: In diethyl ether; toluene; under inert atm.; Ti complex dissolved in toluene; soln. of MeLi in ether added dropwise with stirring over 1 min; soln. stirred for 45 min; volatiles removed (vac.); residue extd. (hot hexane); soln. filtered hot; put into freezer overnight; solvent decanted; crystals washed (cold hexane); dried (vac.); elem. anal.;
DOI:10.1021/ja070061y