N-[(phenylmethoxy)carbonyl]-L-proline-(1S)-1-[[(2S,3S)-3-hexyl-4-oxo-2-oxetanyl]methyl]dodecyl ester

Base Information

Chemical Name:N-[(phenylmethoxy)carbonyl]-L-proline-(1S)-1-[[(2S,3S)-3-hexyl-4-oxo-2-oxetanyl]methyl]dodecyl ester
CAS No.:1072902-89-6
Molecular Formula:C₃₅H₅₅NO₆
Molecular Weight:585.825
Hs Code.:

Synonyms:N-[(phenylmethoxy)carbonyl]-L-proline-(1S)-1-[[(2S,3S)-3-hexyl-4-oxo-2-oxetanyl]methyl]dodecyl ester

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Chemical Property of N-[(phenylmethoxy)carbonyl]-L-proline-(1S)-1-[[(2S,3S)-3-hexyl-4-oxo-2-oxetanyl]methyl]dodecyl ester

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Technology Process of N-[(phenylmethoxy)carbonyl]-L-proline-(1S)-1-[[(2S,3S)-3-hexyl-4-oxo-2-oxetanyl]methyl]dodecyl ester

There total 3 articles about N-[(phenylmethoxy)carbonyl]-L-proline-(1S)-1-[[(2S,3S)-3-hexyl-4-oxo-2-oxetanyl]methyl]dodecyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 104871-99-0,104872-00-6,104872-03-9,104872-05-1,104872-06-2,104872-07-3,104872-19-7,68711-40-0
(3S,4S)-3-hexyl-4-[(2S)-2-hydroxytridecyl]oxetan-2-one

: 1148-11-4
N-Benzyloxycarbonyl-L-proline

: 1072902-89-6
N-[(phenylmethoxy)carbonyl]-L-proline-(1S)-1-[[(2S,3S)-3-hexyl-4-oxo-2-oxetanyl]methyl]dodecyl ester

Guidance literature:: With dmap; diisopropyl-carbodiimide; In N,N-dimethyl-formamide; at 0 - 25 ℃; for 72h; Inert atmosphere;
DOI:10.1039/c0cc05635a

Reference yield:

: 1072902-83-0
(2S,3S,5S)-2-hexyl-3-hydroxy-5-((triisopropylsilyl)oxy)hexadecanoic acid

: 1072902-89-6
N-[(phenylmethoxy)carbonyl]-L-proline-(1S)-1-[[(2S,3S)-3-hexyl-4-oxo-2-oxetanyl]methyl]dodecyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; benzenesulfonyl chloride / 48.4 h / -18 - 0 °C

2: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 15.25 h / -20 - -18 °C

3: dmap; diisopropyl-carbodiimide / N,N-dimethyl-formamide / 72 h / 0 - 25 °C / Inert atmosphere

With pyridine; dmap; tetrabutyl ammonium fluoride; acetic acid; benzenesulfonyl chloride; diisopropyl-carbodiimide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/c0cc05635a

Reference yield:

: 1072902-84-1
(3S,4S)-3-hexyl-4-[(2S)-2-[(triisopropylsilyl)oxy]tridecyl]oxetan-2-one

: 1072902-89-6
N-[(phenylmethoxy)carbonyl]-L-proline-(1S)-1-[[(2S,3S)-3-hexyl-4-oxo-2-oxetanyl]methyl]dodecyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 15.25 h / -20 - -18 °C

2: dmap; diisopropyl-carbodiimide / N,N-dimethyl-formamide / 72 h / 0 - 25 °C / Inert atmosphere

With dmap; tetrabutyl ammonium fluoride; acetic acid; diisopropyl-carbodiimide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/c0cc05635a