(3S,4S)-3-Hexyl-4[(S)-2-(triisopropylsilyloxy)tridecyl]-2-oxetanone

Base Information

Chemical Name:(3S,4S)-3-Hexyl-4[(S)-2-(triisopropylsilyloxy)tridecyl]-2-oxetanone
CAS No.:1072902-84-1
Molecular Formula:C₃₁H₆₂O₃Si
Molecular Weight:510.917
Hs Code.:
Mol file:1072902-84-1.mol

Synonyms:(3S,4S)-3-hexyl-4-[(2S)-2-[(triisopropylsilyl)oxy]tridecyl]oxetan-2-one

Suppliers and Price of (3S,4S)-3-Hexyl-4[(S)-2-(triisopropylsilyloxy)tridecyl]-2-oxetanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
(3S,4S)-3-Hexyl-4[(S)-2-(triisopropylsilyloxy)tridecyl]-2-oxetanone
10mg
$ 1270.00

Total 2 raw suppliers

Chemical Property of (3S,4S)-3-Hexyl-4[(S)-2-(triisopropylsilyloxy)tridecyl]-2-oxetanone

Chemical Property:

Boiling Point:540.7±23.0 °C(Predicted)
Density:0.890±0.06 g/cm3(Predicted)
Storage Temp.:Hygroscopic, Refrigerator, under inert atmosphere
Solubility.:Chloroform (Slightly), Ethyl Acetate (Slightly)

Purity/Quality:

96% ^*data from raw suppliers

(3S,4S)-3-Hexyl-4[(S)-2-(triisopropylsilyloxy)tridecyl]-2-oxetanone ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Uses A reagent used in the synthesis of enzymatic endocannabinoid 2-arachidonoylglycerol hydrolysis inhibitors and respective analogs (3S,4S)-3-Hexyl-4[(S)-2-(triisopropylsilyloxy)tridecyl]-2-oxetanone is a reagent used in the synthesis of enzymatic endocannabinoid 2-arachidonoylglycerol hydrolysis inhibitors and respective analogs

Technology Process of (3S,4S)-3-Hexyl-4[(S)-2-(triisopropylsilyloxy)tridecyl]-2-oxetanone

There total 5 articles about (3S,4S)-3-Hexyl-4[(S)-2-(triisopropylsilyloxy)tridecyl]-2-oxetanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1072902-83-0
(2S,3S,5S)-2-hexyl-3-hydroxy-5-((triisopropylsilyl)oxy)hexadecanoic acid

: 1072902-84-1
(3S,4S)-3-hexyl-4-[(2S)-2-[(triisopropylsilyl)oxy]tridecyl]oxetan-2-one

Guidance literature:: With N,N-phenylbistrifluoromethane-sulfonimide; triethylamine; In dichloromethane; for 16h;
DOI:10.1016/j.ejmech.2021.113358

Reference yield: 63.2%

: 1072902-82-9
(2S,3S,5S)-2-hexyl-5-hydroxy-3-[(triisopropylsilyl)oxy]hexadecanoic acid phenylmethyl ester

: 1072902-84-1
(3S,4S)-3-hexyl-4-[(2S)-2-[(triisopropylsilyl)oxy]tridecyl]oxetan-2-one

Guidance literature:: (2S,3S,5S)-2-hexyl-5-hydroxy-3-[(triisopropylsilyl)oxy]hexadecanoic acid phenylmethyl ester; With palladium 10% on activated carbon; hydrogen; In ethyl acetate; at 20 ℃; under 760.051 Torr;

With N,N-phenylbistrifluoromethane-sulfonimide; triethylamine; Inert atmosphere;

Reference yield:

: (2S,3S,5S)-3,5-dihydroxy-2-hexylhexadecanoic acid phenylmethyl ester

: 1072902-84-1
(3S,4S)-3-hexyl-4-[(2S)-2-[(triisopropylsilyl)oxy]tridecyl]oxetan-2-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: 2,4,6-trimethyl-pyridine / dichloromethane / 3 h / -78 °C / Inert atmosphere

2.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 20 °C / 760.05 Torr

2.2: Inert atmosphere

With 2,4,6-trimethyl-pyridine; palladium 10% on activated carbon; hydrogen; In dichloromethane; ethyl acetate;