α-isopropyl-3,4,5-trimethoxy-α-<2--N-methylamino>ethyl>benzeneacetonitrile

Base Information

Chemical Name:α-isopropyl-3,4,5-trimethoxy-α-<2--N-methylamino>ethyl>benzeneacetonitrile
CAS No.:103524-03-4
Molecular Formula:C₂₆H₃₆N₂O₅
Molecular Weight:456.582
Hs Code.:

α-isopropyl-3,4,5-trimethoxy-α-<2-<N-<2-(2-methoxyphenoxy)ethyl>-N-methylamino>ethyl>benzeneacetonitrile

Synonyms:α-isopropyl-3,4,5-trimethoxy-α-<2--N-methylamino>ethyl>benzeneacetonitrile

Suppliers and Price of α-isopropyl-3,4,5-trimethoxy-α-<2--N-methylamino>ethyl>benzeneacetonitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of α-isopropyl-3,4,5-trimethoxy-α-<2--N-methylamino>ethyl>benzeneacetonitrile

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of α-isopropyl-3,4,5-trimethoxy-α-<2--N-methylamino>ethyl>benzeneacetonitrile

There total 5 articles about α-isopropyl-3,4,5-trimethoxy-α-<2--N-methylamino>ethyl>benzeneacetonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 103524-02-3
α-isopropyl-3,4,5-trimethoxy-α-<2-<<2-(2-methoxyphenoxy)ethyl>amino>ethyl>benzeneacetonitrile

: 103524-03-4
α-isopropyl-3,4,5-trimethoxy-α-<2--N-methylamino>ethyl>benzeneacetonitrile

Guidance literature:: With oxalic acid; In water; at 90 ℃; for 1h;
DOI:10.1248/cpb.36.367

Reference yield:

: 1836-62-0
2-(2-methoxy-phenoxy)-ethylamine

: 103524-03-4
α-isopropyl-3,4,5-trimethoxy-α-<2--N-methylamino>ethyl>benzeneacetonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 2.) NaBH₄ / 1.) MeOH, 1 H, reflux, 2.) MeOH, ice water, 1 h, room temp.

2: 84 percent / oxalic acid / H₂O / 1 h / 90 °C

With sodium tetrahydroborate; oxalic acid; In water;
DOI:10.1248/cpb.36.367

Reference yield:

: 36622-33-0
α-isopropyl-3,4,5-trimethoxybenzenacetonitrilie

: 103524-03-4
α-isopropyl-3,4,5-trimethoxy-α-<2--N-methylamino>ethyl>benzeneacetonitrile

Guidance literature:: Multi-step reaction with 4 steps

1: 78.00 g / tetrahydrofuran / 4 h / Heating

2: 62.20 g / 10percent (COOH)2 / acetone; H₂O / 6 h / Heating

3: 2.) NaBH₄ / 1.) MeOH, 1 H, reflux, 2.) MeOH, ice water, 1 h, room temp.

4: 84 percent / oxalic acid / H₂O / 1 h / 90 °C

With sodium tetrahydroborate; oxalic acid; In tetrahydrofuran; water; acetone;
DOI:10.1248/cpb.36.367