2-(3-Iodophenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Base Information

Chemical Name:2-(3-Iodophenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
CAS No.:408492-28-4
Molecular Formula:C12H16 B I O2
Molecular Weight:329.973
Hs Code.:2931900090
European Community (EC) Number:622-737-2
DSSTox Substance ID:DTXSID10462094
Nikkaji Number:J1.689.016B
Mol file:408492-28-4.mol

Synonyms:408492-28-4;2-(3-iodophenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane;3-IODOPHENYLBORONIC ACID PINACOL ESTER;3-Iodophenylboronic acid, pinacol ester;MFCD09953498;3-Iodo-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzene;3-Iodophenylboronic acid pinacolester;3-Iodophenylboronic acid pinacol ester, 97%;SCHEMBL15403788;DTXSID10462094;AKOS005259446;AS-2323;3-Iodophenylboronic acid pinacol ester,97%;CS-0168637;3-Iodobenzeneboronic acid pinacol ester, 97%;E79077;A821941;A873210;2-(3-iodanylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Suppliers and Price of 2-(3-Iodophenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
3-Iodophenylboronic acid pinacol ester
1g
$ 75.00

TRC
3-Iodophenylboronic acid pinacol ester
100mg
$ 45.00

Sigma-Aldrich
3-Iodophenylboronic acid pinacol ester 97%
5g
$ 151.00

Sigma-Aldrich
3-Iodophenylboronic acid pinacol ester 97%
1g
$ 61.00

Matrix Scientific
3-Iodophenylboronic acid pinacol ester >95%
500mg
$ 67.00

Matrix Scientific
3-Iodophenylboronic acid pinacol ester >95%
1g
$ 90.00

Matrix Scientific
3-Iodophenylboronic acid pinacol ester >95%
5g
$ 264.00

Crysdot
2-(3-Iodophenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane 95+%
25g
$ 452.00

AOBChem
3-Iodophenylboronic acid pinacol ester 95%
5g
$ 117.00

AOBChem
3-Iodophenylboronic acid pinacol ester 95%
10g
$ 200.00

Total 22 raw suppliers

Chemical Property of 2-(3-Iodophenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Chemical Property:

Melting Point:70-72°C
PSA：18.46000
LogP:2.59040
Sensitive.:Light Sensitive
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:330.02881
Heavy Atom Count:16
Complexity:252

Purity/Quality:

97% ^*data from raw suppliers

3-Iodophenylboronic acid pinacol ester ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:Xn
Statements: 22

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Canonical SMILES:B1(OC(C(O1)(C)C)(C)C)C2=CC(=CC=C2)I
Uses 3-Iodophenylboronic acid, pinacol ester

Technology Process of 2-(3-Iodophenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

There total 12 articles about 2-(3-Iodophenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 76-09-5
2,3-dimethyl-2,3-butane diol

: 221037-98-5
(3-iodophenyl)boronic acid

: 408492-28-4
2-(3-iodo-phenyl)-4,4,5,5-tetramethyl[1,3,2]dioxaborolane

Guidance literature:: With calcium sulfate; In toluene; for 3.5h; Reflux;

Reference yield: 88.0%

: 626-00-6
1,3-Diiodobenzene

: 1195-66-0
2-methoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 408492-28-4
2-(3-iodo-phenyl)-4,4,5,5-tetramethyl[1,3,2]dioxaborolane

Guidance literature:: 1,3-Diiodobenzene; With TurboGrignard; In tetrahydrofuran; at -20 ℃; for 1h;

2-methoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane; In tetrahydrofuran; at -20 - 20 ℃;
DOI:10.1002/anie.200462928