thymidine-5'-aspartyl phosphoramidate

Base Information

• Chemical Name: thymidine-5'-aspartyl phosphoramidate
• CAS No.: 1052236-38-0
• Molecular Formula: C₁₄H₂₀N₃O₁₁P
• Molecular Weight: 437.3

Synonyms:thymidine-5'-aspartyl phosphoramidate

Chemical Property of thymidine-5'-aspartyl phosphoramidate

Chemical Property:

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Technology Process of thymidine-5'-aspartyl phosphoramidate

There total 1 articles about thymidine-5'-aspartyl phosphoramidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

thymidine 5'-phosphate (365-07-1,15108-71-1,60363-32-8,96744-88-6,132696-16-3,143838-77-1) → thymidine-5'-aspartyl phosphoramidate (1052236-38-0)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine; dicyclohexyl-carbodiimide / water; tert-butyl alcohol / 95 °C / Inert atmosphere

2: water; sodium hydroxide / methanol / 20 °C / pH Ca_. 7.5 / Inert atmosphere; aq. acetate buffer

With water; triethylamine; dicyclohexyl-carbodiimide; sodium hydroxide; In methanol; water; tert-butyl alcohol;

DOI:10.1002/chem.201102279

upstream raw materials:

thymidine 5'-phosphate

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