1-acetyl-6-chloro-3,4-dihydro-3-methyl-4-phenyl-4-trichloromethyl-2(1H)-quinazolinone

Base Information

Chemical Name:1-acetyl-6-chloro-3,4-dihydro-3-methyl-4-phenyl-4-trichloromethyl-2(1H)-quinazolinone
CAS No.:80170-89-4
Molecular Formula:C₁₈H₁₄Cl₄N₂O₂
Molecular Weight:432.133
Hs Code.:

Synonyms:1-acetyl-6-chloro-3,4-dihydro-3-methyl-4-phenyl-4-trichloromethyl-2(1H)-quinazolinone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-acetyl-6-chloro-3,4-dihydro-3-methyl-4-phenyl-4-trichloromethyl-2(1H)-quinazolinone

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Technology Process of 1-acetyl-6-chloro-3,4-dihydro-3-methyl-4-phenyl-4-trichloromethyl-2(1H)-quinazolinone

There total 5 articles about 1-acetyl-6-chloro-3,4-dihydro-3-methyl-4-phenyl-4-trichloromethyl-2(1H)-quinazolinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 108-24-7
acetic anhydride

: 80170-53-2
6-chloro-3,4-dihydro-3-methyl-4-phenyl-4-trichloromethyl-2(1H)-quinazolinone

: 80170-89-4
1-acetyl-6-chloro-3,4-dihydro-3-methyl-4-phenyl-4-trichloromethyl-2(1H)-quinazolinone

Guidance literature:: for 6h; Heating;
DOI:10.1248/cpb.29.2135

Reference yield:

: 26381-66-8
5-chloro-2-trichloroacetylaminobenzophenone

: 80170-89-4
1-acetyl-6-chloro-3,4-dihydro-3-methyl-4-phenyl-4-trichloromethyl-2(1H)-quinazolinone

Guidance literature:: Multi-step reaction with 5 steps

1: 16 percent / ethanol / 3 h / 60 °C

2: TiCl₄ / benzene

3: 55 percent / triethylamine / benzene / 2 h / Ambient temperature

4: 87 percent / NaHCO₃ / dimethylformamide / 4 h / Ambient temperature

5: 74 percent / 6 h / Heating

With titanium tetrachloride; sodium hydrogencarbonate; triethylamine; In ethanol; N,N-dimethyl-formamide; benzene;
DOI:10.1248/cpb.29.2135

Reference yield:

: 719-59-5
5-chloro-2-aminobenzophenone

: 80170-89-4
1-acetyl-6-chloro-3,4-dihydro-3-methyl-4-phenyl-4-trichloromethyl-2(1H)-quinazolinone

Guidance literature:: Multi-step reaction with 4 steps

1: TiCl₄ / benzene

2: 55 percent / triethylamine / benzene / 2 h / Ambient temperature

3: 87 percent / NaHCO₃ / dimethylformamide / 4 h / Ambient temperature

4: 74 percent / 6 h / Heating

With titanium tetrachloride; sodium hydrogencarbonate; triethylamine; In N,N-dimethyl-formamide; benzene;
DOI:10.1248/cpb.29.2135