C₂₄H₂₁Cl₂NO₆

Base Information

Chemical Name:C₂₄H₂₁Cl₂NO₆
CAS No.:1611455-47-0
Molecular Formula:C₂₄H₂₁Cl₂NO₆
Molecular Weight:490.34
Hs Code.:

C<sub>24</sub>H<sub>21</sub>Cl<sub>2</sub>NO<sub>6</sub>

Synonyms:C₂₄H₂₁Cl₂NO₆

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Chemical Property of C₂₄H₂₁Cl₂NO₆

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Technology Process of C₂₄H₂₁Cl₂NO₆

There total 8 articles about C₂₄H₂₁Cl₂NO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1611455-46-9
[(1S)-2-(3,5-dichloro-1-oxido-pyridin-1-ium-4-yl)-1-(3,4-dimethoxyphenyl)-ethyl]-4-(1,3-dioxolan-2-ylmethyl)benzoate

: 1611455-47-0
C₂₄H₂₁Cl₂NO₆

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; water; at 40 ℃;

Reference yield:

: 120-14-9
3,4-dimethoxy-benzaldehyde

: 1611455-47-0
C₂₄H₂₁Cl₂NO₆

Guidance literature:: Multi-step reaction with 7 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

1.2: -78 °C

2.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 2 h / 20 °C

3.1: methanol; chloroform / 2 h / 20 °C

4.1: potassium tert-butylate; methanol / toluene / 24 h / 20 °C

5.1: 3-chloro-benzenecarboperoxoic acid / ethyl acetate / 5 h / 20 °C

6.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 18 h / 20 °C

7.1: hydrogenchloride / tetrahydrofuran; water / 40 °C

With hydrogenchloride; methanol; dmap; potassium tert-butylate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 3-chloro-benzenecarboperoxoic acid; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; dichloromethane; chloroform; water; ethyl acetate; N,N-dimethyl-formamide; toluene;

Reference yield:

: 1113061-23-6
(R,S)-2-(3,5-dichloropyridin-4-yl)-1-(3,4-dimethoxyphenyl)ethanol

: 1611455-47-0
C₂₄H₂₁Cl₂NO₆

Guidance literature:: Multi-step reaction with 6 steps

1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 2 h / 20 °C

2: methanol; chloroform / 2 h / 20 °C

3: potassium tert-butylate; methanol / toluene / 24 h / 20 °C

4: 3-chloro-benzenecarboperoxoic acid / ethyl acetate / 5 h / 20 °C

5: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 18 h / 20 °C

6: hydrogenchloride / tetrahydrofuran; water / 40 °C

With hydrogenchloride; methanol; dmap; potassium tert-butylate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; dichloromethane; chloroform; water; ethyl acetate; N,N-dimethyl-formamide; toluene;