8-(3,4-dichlorophenyl)-2-[3-methoxy-4-(2-methyl-1,3-oxazol-5-yl)phenyl]-5,6,7,8-tetrahydro[1,2,4]triazolo[1,5-a]pyridine

Base Information

Chemical Name:8-(3,4-dichlorophenyl)-2-[3-methoxy-4-(2-methyl-1,3-oxazol-5-yl)phenyl]-5,6,7,8-tetrahydro[1,2,4]triazolo[1,5-a]pyridine
CAS No.:1262106-21-7
Molecular Formula:C₂₃H₂₀Cl₂N₄O₂
Molecular Weight:455.343
Hs Code.:

Synonyms:8-(3,4-dichlorophenyl)-2-[3-methoxy-4-(2-methyl-1,3-oxazol-5-yl)phenyl]-5,6,7,8-tetrahydro[1,2,4]triazolo[1,5-a]pyridine

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Chemical Property of 8-(3,4-dichlorophenyl)-2-[3-methoxy-4-(2-methyl-1,3-oxazol-5-yl)phenyl]-5,6,7,8-tetrahydro[1,2,4]triazolo[1,5-a]pyridine

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Technology Process of 8-(3,4-dichlorophenyl)-2-[3-methoxy-4-(2-methyl-1,3-oxazol-5-yl)phenyl]-5,6,7,8-tetrahydro[1,2,4]triazolo[1,5-a]pyridine

There total 7 articles about 8-(3,4-dichlorophenyl)-2-[3-methoxy-4-(2-methyl-1,3-oxazol-5-yl)phenyl]-5,6,7,8-tetrahydro[1,2,4]triazolo[1,5-a]pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 1262106-83-1
3-methoxy-4-(2-methyl-1,3-oxazol-5-yl)benzohydrazide hydrochloride

: 1262107-23-2
ethyl 5-chloro-2-(3,4-dichlorophenyl)pentaneimidate hydrochloride

: 1262106-21-7
8-(3,4-dichlorophenyl)-2-[3-methoxy-4-(2-methyl-1,3-oxazol-5-yl)phenyl]-5,6,7,8-tetrahydro[1,2,4]triazolo[1,5-a]pyridine

Guidance literature:: With 1H-imidazole; In methanol; at 20 - 65 ℃; for 19h;

Reference yield: 46.0%

: 1262106-83-1
3-methoxy-4-(2-methyl-1,3-oxazol-5-yl)benzohydrazide hydrochloride

: C₁₃H₁₆Cl₃NO

: 1262106-21-7
8-(3,4-dichlorophenyl)-2-[3-methoxy-4-(2-methyl-1,3-oxazol-5-yl)phenyl]-5,6,7,8-tetrahydro[1,2,4]triazolo[1,5-a]pyridine

Guidance literature:: With 1H-imidazole; In methanol; at 20 - 65 ℃;
DOI:10.1016/j.bmcl.2015.07.101

Reference yield:

: 1262107-24-3
5-chloro-2-(3,4-dichlorophenyl)pentanenitrile

: 1262106-21-7
8-(3,4-dichlorophenyl)-2-[3-methoxy-4-(2-methyl-1,3-oxazol-5-yl)phenyl]-5,6,7,8-tetrahydro[1,2,4]triazolo[1,5-a]pyridine

Guidance literature:: Multi-step reaction with 2 steps

1: acetyl chloride / ethanol / 60 h / 20 °C / Cooling with ice

2: 1H-imidazole / methanol / 19 h / 20 - 65 °C

With 1H-imidazole; acetyl chloride; In methanol; ethanol;