2-(3-bromophenyl)-1,1-diethylhydrazine

Base Information

• Chemical Name: 2-(3-bromophenyl)-1,1-diethylhydrazine
• CAS No.: 114838-65-2
• Molecular Formula: C₁₀H₁₅BrN₂
• Molecular Weight: 243.146
• Mol file: 114838-65-2.mol

Synonyms:

Chemical Property of 2-(3-bromophenyl)-1,1-diethylhydrazine

Chemical Property:

• Vapor Pressure: 0.00513mmHg at 25°C
• Boiling Point: 275.3°Cat760mmHg
• Flash Point: 120.3°C
• Density: 1.337g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-(3-bromophenyl)-1,1-diethylhydrazine

There total 6 articles about 2-(3-bromophenyl)-1,1-diethylhydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

N-(3-bromophenyl)-N-hydroxy-2,2-dimethylpropanamide (114838-67-4) + diethylamine (109-89-7) → N'-(3-Bromo-phenyl)-N,N-diethyl-hydrazine (114838-65-2)

Guidance literature:

at 55 ℃; for 8h;

Reference yield: 84.0%

N-hydroxy-3-bromoacetanilide (38373-20-5) + diethylamine (109-89-7) → N'-(3-Bromo-phenyl)-N,N-diethyl-hydrazine (114838-65-2)

Guidance literature:

at 55 ℃; for 40h;

Reference yield: 67.0%

N-(3-bromophenyl)-O-pivaloylhydroxylamine (107986-35-6) + diethylamine (109-89-7) → N'-(3-Bromo-phenyl)-N,N-diethyl-hydrazine (114838-65-2) + bis-(3-bromo-phenyl)-diazene-N-oxide (23377-24-4)

Guidance literature:

at 55 ℃; for 0.5h;

upstream raw materials:

N-hydroxy-3-bromoacetanilide

diethylamine

N-(3-bromophenyl)-O-pivaloylhydroxylamine

C₈H₈BrNO₂

Refernces