potassium 5-benzyl-5-(cyclohex-1-en-1-ylmethyl)-4,6-dioxo-1,4,5,6-tetrahydropyrimidine-2-thiolate

Base Information

Chemical Name:potassium 5-benzyl-5-(cyclohex-1-en-1-ylmethyl)-4,6-dioxo-1,4,5,6-tetrahydropyrimidine-2-thiolate
CAS No.:1383550-17-1
Molecular Formula:C₁₈H₁₉N₂O₂S*K
Molecular Weight:366.525
Hs Code.:

Synonyms:potassium 5-benzyl-5-(cyclohex-1-en-1-ylmethyl)-4,6-dioxo-1,4,5,6-tetrahydropyrimidine-2-thiolate

Suppliers and Price of potassium 5-benzyl-5-(cyclohex-1-en-1-ylmethyl)-4,6-dioxo-1,4,5,6-tetrahydropyrimidine-2-thiolate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of potassium 5-benzyl-5-(cyclohex-1-en-1-ylmethyl)-4,6-dioxo-1,4,5,6-tetrahydropyrimidine-2-thiolate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of potassium 5-benzyl-5-(cyclohex-1-en-1-ylmethyl)-4,6-dioxo-1,4,5,6-tetrahydropyrimidine-2-thiolate

There total 4 articles about potassium 5-benzyl-5-(cyclohex-1-en-1-ylmethyl)-4,6-dioxo-1,4,5,6-tetrahydropyrimidine-2-thiolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1383550-10-4
5-benzyl-5-(cyclohexenylmethyl)-2-thioxo-dihydropyrimidine-4,6(1H,5H)-dione

: 1383550-17-1
potassium 5-benzyl-5-(cyclohex-1-en-1-ylmethyl)-4,6-dioxo-1,4,5,6-tetrahydropyrimidine-2-thiolate

Guidance literature:: With potassium hydroxide; In isopropyl alcohol; Inert atmosphere;
DOI:10.3390/molecules17044313

Reference yield:

: 1192-37-6
methylenecyclohexane

: 1383550-17-1
potassium 5-benzyl-5-(cyclohex-1-en-1-ylmethyl)-4,6-dioxo-1,4,5,6-tetrahydropyrimidine-2-thiolate

Guidance literature:: Multi-step reaction with 3 steps

1: copper(II) acetate monohydrate; manganese(III) triacetate dihydrate; acetic acid / 1 h / 60 - 80 °C / Microwave irradiation

2: potassium tert-butylate / dimethyl sulfoxide / 4 h / 50 °C / Inert atmosphere

3: potassium hydroxide / isopropyl alcohol / Inert atmosphere

With potassium tert-butylate; copper(II) acetate monohydrate; manganese(III) triacetate dihydrate; acetic acid; potassium hydroxide; In dimethyl sulfoxide; isopropyl alcohol;
DOI:10.3390/molecules17044313

Reference yield:

: 1374015-50-5
diethyl 2-benzyl-2-(cyclohexenylmethyl)malonate

: 1383550-17-1
potassium 5-benzyl-5-(cyclohex-1-en-1-ylmethyl)-4,6-dioxo-1,4,5,6-tetrahydropyrimidine-2-thiolate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium tert-butylate / dimethyl sulfoxide / 4 h / 50 °C / Inert atmosphere

2: potassium hydroxide / isopropyl alcohol / Inert atmosphere

With potassium tert-butylate; potassium hydroxide; In dimethyl sulfoxide; isopropyl alcohol;
DOI:10.3390/molecules17044313