methyl 4-(acetylamino)-3-<acetyl>benzoate

Base Information

Chemical Name:methyl 4-(acetylamino)-3-<acetyl>benzoate
CAS No.:164466-92-6
Molecular Formula:C₂₀H₂₁N₃O₆
Molecular Weight:399.403
Hs Code.:

methyl 4-(acetylamino)-3-<<N-(benzyloxycarbonyl)amino>acetyl>benzoate

Synonyms:methyl 4-(acetylamino)-3-<acetyl>benzoate

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Chemical Property of methyl 4-(acetylamino)-3-<acetyl>benzoate

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Technology Process of methyl 4-(acetylamino)-3-<acetyl>benzoate

There total 3 articles about methyl 4-(acetylamino)-3-<acetyl>benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1138-80-3
N-(Benzyloxycarbonyl)glycine

: 84445-93-2
methyl 4-(acetylamino)-3-aminobenzoate

: 164466-92-6
methyl 4-(acetylamino)-3-<acetyl>benzoate

Guidance literature:: With dicyclohexyl-carbodiimide; In 1,4-dioxane; N,N-dimethyl-formamide; for 4h; Ambient temperature;
DOI:10.1021/jm00017a005

Reference yield:

: 1539-06-6
3-nitro-4-acetamidobenzoic acid

: 164466-92-6
methyl 4-(acetylamino)-3-<acetyl>benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 94.3 percent / diisopropylethylamine / dimethylformamide / 24 h / Ambient temperature

2: 78.7 percent / 5percent HCl, hydrazine hydrate / 10percent Pd/C / ethanol / 1 h / Ambient temperature

3: 68 percent / DCC / dimethylformamide; dioxane / 4 h / Ambient temperature

With hydrogenchloride; hydrazine hydrate; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In 1,4-dioxane; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00017a005

Reference yield:

: 6313-39-9
4-acetamido-3-nitro-benzoic acid methyl ester

: 164466-92-6
methyl 4-(acetylamino)-3-<acetyl>benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 78.7 percent / 5percent HCl, hydrazine hydrate / 10percent Pd/C / ethanol / 1 h / Ambient temperature

2: 68 percent / DCC / dimethylformamide; dioxane / 4 h / Ambient temperature

With hydrogenchloride; hydrazine hydrate; dicyclohexyl-carbodiimide; palladium on activated charcoal; In 1,4-dioxane; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00017a005